Carbon monoxide releasing molecule with up-conversion nano-phosphor, method for preparing carbon monoxide releasing molecule and application thereof
A luminescent material, carbon monoxide technology, applied in luminescent materials, chemical instruments and methods, wave energy or particle radiation treatment materials, etc., can solve the problem of difficult to induce PhotoCORMs to release CO, achieve good up-conversion luminescence characteristics, broad application prospects, Simple steps to synthesize effects
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Embodiment 1
[0035] 1. A preparation method of an up-conversion luminescent material carbon monoxide release agent
[0036] (1) Preparation of UCNPs nanomaterials
[0037] At room temperature, take the precursor (LnCl 3 , Ln 3+ =Y 3+ , Yb 3+ , Er 3+ ; molar ratio Y 3+ :Yb 3+ :Er 3+ =78:20:2) 2mL, 6mL of oleic acid, 15mL of 1-octadecene were added to a 100mL three-necked flask, stirred and mixed evenly, then the temperature was raised to 50°C and kept for 20min, then raised to 140°C and kept at this temperature 60min. After natural cooling to 30°C, 10mL methanol (dissolved with 2.5mmol NaOH, 4mmol NH 4 F) Add dropwise to the reaction solution, and after 10 minutes, raise the temperature to 70° C. to remove methanol. Finally, argon was passed and degassed at 100 °C for 10 min, then the temperature was rapidly raised to 320 °C and the reaction was carried out at this temperature for 60 min to generate upconversion nanoparticles UCNPs. After washing with ethanol, UCNPs were disperse...
Embodiment 2
[0047] 1. A preparation method of an up-conversion luminescent material carbon monoxide release agent
[0048] (1) Preparation of UCNPs nanomaterials
[0049] At room temperature, take the precursor (LnCl 3 , Ln 3+ =Y 3+ , Yb 3+ , Er 3+ ; molar ratio Y 3+ :Yb 3+ :Er 3+ =78:20:2) 2mL, oleic acid 10mL, 1-octadecene 20mL were added to a 100mL three-necked flask, stirred and mixed evenly, then the temperature was raised to 50°C and kept for 20min, then raised to 140°C and kept at this temperature 60min. After natural cooling to 30°C, 10mL methanol (dissolved with 2.5mmol NaOH, 4mmol NH 4 F) Add dropwise to the reaction solution, and after 10 minutes, raise the temperature to 70° C. to remove methanol. Finally, argon was passed and degassed at 100 °C for 10 min, then the temperature was rapidly raised to 300 °C and the reaction was carried out at this temperature for 90 min to generate upconversion nanoparticles UCNPs. UCNPs were washed with ethanol and dispersed in cycl...
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