Chlorine evolution accelerator and preparation method thereof
An accelerator and chlorine analysis technology, which is applied in chemical instruments and methods, physical/chemical process catalysts, electrodes, etc., can solve problems such as secondary pollution, high operating costs, and complicated operations, so as to improve equipment production capacity and chlorine analysis efficiency The effect of increasing and improving the efficiency of chlorine analysis
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Embodiment 1-5
[0051] In embodiment 1-5, the molar percentage composition of each component ion and ion is shown in the table below:
[0052] Table 1 embodiment 1-5 component and proportioning ratio
[0053] Nd 3+
Eu 3+
Yb 3+
Gd 3+
Dy 3+
Example 1 25mol% 15mol% 60mol% - - Example 2 - - 40mol% 40mol% 20mol% Example 3 - 25mol% - 45mol% 30mol% Example 4 30mol% 30mol% - 20mol% 20mol% Example 5 25mol% 35mol% 25mol% - 15mol%
[0054] - Indicates that it does not contain this component
[0055] Wherein, the neodymium ion of embodiment 1 comes from neodymium chloride, neodymium nitrate, europium ion comes from europium chloride, europium nitrate, ytterbium ion comes from ytterbium sulfate, ytterbium carbonate; The ytterbium ion of embodiment 2 comes from ytterbium nitrate, gadolinium ion comes from chloride Gadolinium, gadolinium nitrate, gadolinium sulfate, and dysprosium ion are from dys...
experiment example
[0058] The chlorine analysis accelerators of Examples 1-5 were introduced into the electrodes of the sodium hypochlorite generator, and the chlorine analysis reaction and the chlorine analysis efficiency of the sodium hypochlorite generator electrodes were tested.
[0059] The experimental steps are as follows:
[0060] (1) Use a titanium plate with a titanium content of 99.9% and a thickness of 1 mm as the substrate. After the titanium plate is sandblasted and polished to remove the oxide layer, it is placed in a NaOH solution with a concentration of 10% and shaken for 30 minutes, and then the oxalic acid with a concentration of 20% The solution etches the titanium plate for 2 hours, and after cleaning, place it in an ethanol solution for use;
[0061](2) Preparation of active coating liquid: use n-butanol: isopropanol = 2:1 mixed solution as solvent, ruthenium trichloride, chloroiridic acid, tetrabutyl titanate, chlorine evolution accelerator as solute, and Concentrated hyd...
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