Production method of attapulgite suspending agent
A production method, the attapulgite technology, applied in the direction of coating, etc., can solve the problems of expensive raw materials of bentonite, poor anti-settling effect of organic bentonite, exhaustion of high-quality bentonite resources, etc., and achieve excellent adsorption and bonding performance and anti-settling effect Good, conducive to the effect of modification
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Embodiment 1
[0022] A production method of attapulgite suspension, comprising the steps of:
[0023] (1) Purification of attapulgite clay: After drying the attapulgite raw ore outdoors for 2-3 days, crush it, wash it with water 10 times the mass of the attapulgite raw ore, filter and bake the filtrate at 60°C for 3 hours to obtain purified attapulgite clay ;
[0024] (2) Acidification treatment: Slowly add 49% sulfuric acid to the purified attapulgite clay to a pH value of 5.5-6.5, and stir at a speed of 40-60 rpm while adding it, and after stirring for 20-30 minutes, Add an ethanol solvent 25 times the mass of the purified attapulgite clay, and continue stirring for 30-40 minutes at 600-800 rpm;
[0025] (3) Suspension preparation: Mix the reaction solution in step (2) with silicon dioxide, tetrabutylammonium bromide, and sodium carboxymethylcellulose, heat up to 30-40°C and stir for 20 minutes, then ultrasonically treat at 15KHz for 30 minutes. Minutes, milky white slurry is obtained, ...
Embodiment 2
[0027] A production method of attapulgite suspension, comprising the steps of:
[0028] (1) Purification of attapulgite clay: After drying the attapulgite raw ore outdoors for 2-3 days, crush it, wash it with water 12 times the mass of the attapulgite raw ore, filter and bake the filtrate at 70°C for 2.5 hours to obtain purified attapulgite clay ;
[0029] (2) Acidification treatment: Slowly add 49% sulfuric acid to the purified attapulgite clay to a pH value of 5.5-6.5, and stir at a speed of 40-60 rpm while adding it, and after stirring for 20-30 minutes, Add an ethanol solvent 26 times the mass of the purified attapulgite clay, and continue stirring for 30-40 minutes at 600-800 rpm;
[0030] (3) Suspension preparation: Mix the reaction solution in step (2) with silicon dioxide, tetrabutylammonium bromide, and sodium carboxymethylcellulose, heat up to 30-40°C and stir for 20 minutes, then ultrasonically treat at 20KHz for 26 Minutes, milky white slurry is obtained, the slu...
Embodiment 3
[0032] A production method of attapulgite suspension, comprising the steps of:
[0033] (1) Purification of attapulgite clay: After drying the attapulgite raw ore outdoors for 2-3 days, crush it, wash it with water 12 times the mass of the attapulgite raw ore, and dry the filtrate at 80°C for 2 hours after filtration to obtain purified attapulgite clay ;
[0034] (2) Acidification treatment: Slowly add 49% sulfuric acid to the purified attapulgite clay to a pH value of 5.5-6.5, and stir at a speed of 40-60 rpm while adding it, and after stirring for 20-30 minutes, Add an ethanol solvent 26 times the mass of the purified attapulgite clay, and continue stirring for 30-40 minutes at 600-800 rpm;
[0035] (3) Suspension preparation: Mix the reaction solution in step (2) with silicon dioxide, tetrabutylammonium bromide, and sodium carboxymethyl cellulose, heat up to 30-40°C and stir for 20 minutes, then ultrasonicate at 18KHz for 20 minutes. Minutes, milky white slurry is obtaine...
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