Preparation method of metal drawing lubricant
A metal wire drawing and lubricant technology, used in lubricating compositions, petroleum industry, etc., can solve problems such as harming the environment and human health, reducing friction coefficient, metal wire breakage, etc., achieving strong cleaning ability, reducing load, and reducing friction. Effect
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example 1
[0018]First, measure 100mL methyl ricinoleate and 5.5mL formic acid, put them into the reaction kettle, stir at 300r / min for 10min, and heat to 50°C, then add 50mL of 20% hydrogen peroxide solution dropwise at 1mL / min , continue to stir and heat to 60°C, react for 5h, then stand to separate layers, take the upper oil phase, and wash the upper oil phase with 5% sodium carbonate solution until the washing liquid is neutral, and then distill it off under reduced pressure low boilers to obtain epoxy castor oil; then measure 60mL of the above epoxy castor oil, 150mL of isooctyl alcohol, 4g of catalyst D001 resin, put them into a reaction kettle, stir at 300r / min for 15min, and heat to 80°C, constant temperature React for 3 hours to obtain the base oil, then wash the base oil with deionized water and 2% sodium hydroxide solution in turn until the washing liquid is neutral, to obtain a lubricating oil base oil, set aside; then weigh 5g of molybdenum disulfide Powder, 1.5g sodium chol...
example 2
[0021] First measure 110mL of methyl ricinoleate and 5.8mL of formic acid into the reaction kettle, stir at 350r / min for 13min, and heat to 55°C, then add dropwise 55mL of 20% hydrogen peroxide solution at 1mL / min , continue to stir and heat to 65°C, react for 5h, then stand to separate layers, take the upper oil phase, and wash the upper oil phase with 5% sodium carbonate solution until the washing liquid is neutral, then distill it off under reduced pressure low boilers to obtain epoxy castor oil; then measure 70mL of the above epoxy castor oil, 165mL of isooctyl alcohol, 4g of catalyst D001 resin, put them into a reaction kettle, stir at 350r / min for 18min, and heat to 85°C, constant temperature React for 4 hours to obtain the base oil, then wash the base oil with deionized water and 2% sodium hydroxide solution in turn until the washing liquid is neutral, to obtain a lubricating oil base oil, and set aside; then weigh 5g of molybdenum disulfide Powder, 1.6g of sodium chola...
example 3
[0024] First, measure 120mL of methyl ricinoleate and 6.0mL of formic acid into the reactor, stir at 400r / min for 15min, and heat to 60°C, then add dropwise 60mL of 20% hydrogen peroxide solution at 2mL / min , continue to stir and heat to 70°C, react for 6h, then stand for stratification, take the upper oil phase, and wash the upper oil phase with 5% sodium carbonate solution until the washing liquid is neutral, then distill it off under reduced pressure low boilers to obtain epoxy castor oil; then measure 80mL of the above epoxy castor oil, 180mL of isooctyl alcohol, 5g of catalyst D001 resin, put them into a reaction kettle, stir at 400r / min for 20min, and heat to 90°C, constant temperature React for 5 hours to obtain a base oil, then wash the base oil with deionized water and 2% sodium hydroxide solution in turn until the washing liquid is neutral, and obtain a lubricating oil base oil for subsequent use; then weigh 6g of molybdenum disulfide Powder, 1.8g of sodium cholate, ...
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