Graphite-phase nitrogen carbide nanosheet/cobaltosic oxide nanosheet composite nanomaterial of scale-shaped structure and preparation method and application thereof
A technology of cobalt trioxide nanometer and composite nanomaterials, which is applied in chemical instruments and methods, chemical/physical processes, physical/chemical process catalysts, etc., and can solve the problems of low efficiency of quantum dots, small specific surface area, and few active sites. Achieve excellent photocatalytic performance, large specific surface area, and many sites
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[0026] A two-dimensional g-C 3 N 4 Nanosheets / cobalt tetroxide nanosheets fish-scale structure composite nanomaterials are prepared by hydrothermal method. The steps are as follows:
[0027] g-C 3 N 4 Preparation of nanosheets
[0028] Take 2g of melamine powder and spread it on the bottom of a 50 mL crucible, close the lid, and transfer it to the muffle furnace. The temperature is increased to 550 °C at a rate of 2.3 °C / min and kept for 4 h. Then, the temperature is increased at 2.3 °C / min. Speed down to room temperature, get gC 3 N 4 Light yellow powder.
[0029] Take 0.3 g of g-C prepared above 3 N 4 Light yellow powder, add 200 mL deionized water, ultrasonically peel for 6 hours, then centrifuge the solution at 3000 rpm for 5 minutes to remove the unpeeled solid from the lower layer, take out the supernatant and freeze-dry to obtain g-C 3 N 4 Nano flake powder.
[0030] Take 8mg two-dimensional g-C 3 N 4 The nanosheets were fully dissolved in 8 mL of aqueous solution under ultra...
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