Preparation method of high-abundance rare earth sintered neodymium-iron-boron magnet capable of regulating and controlling grain boundary multi-layer structure and product prepared by preparation method
A rare earth neodymium iron boron, multi-layer structure technology, applied in magnetic objects, inductor/transformer/magnet manufacturing, magnetic materials, etc., can solve the problem of single grain boundary strengthening effect, waste of heavy rare earth resources, and inability to fine-tune grain boundary structure question
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Embodiment 1
[0049] This embodiment includes the following steps.
[0050] (1) Preparation of Nd-Fe-B main phase powder with low rare earth content and NdFeB main phase powder containing high abundance rare earth
[0051] When preparing Nd-Fe-B main phase powder with low rare earth content, Nd-Fe-B quick-setting flakes were obtained by smelting and flake rapid cooling. Subsequently, the Nd-Fe-B main phase powder with low rare earth content and an average particle size of about 3.8 μm was obtained through hydrogen explosion and jet milling processes.
[0052] Preparation of NdFeB main phase powder containing high-abundance rare earth, the composition is Nd 12.3 Fe bal B 6.1 and (Nd 10.3 La 2.0 )Fe bal B 3.1 . NdFeB quick-setting flakes are prepared by smelting and flake rapid cooling. Subsequently, through the hydrogen explosion and jet milling process, the NdFeB main phase powder containing high-abundance rare earths with an average particle size of about 3.8 μm was obtained.
[00...
Embodiment 2
[0060] This embodiment includes the following steps.
[0061] (1) Preparation of Nd-Fe-B main phase powder with low rare earth content and NdFeB main phase powder containing high abundance rare earth
[0062] First prepare the Nd-Fe-B main phase powder with low rare earth content, and the NdFeB main phase powder containing high-abundance rare earth (the composition is Nd 12.3 Fe bal B 6.1 and (Nd 10.3 Ce 2.0 )Fe bal B 3.1 ). NdFeB quick-setting flakes are prepared by smelting and flake rapid cooling. Subsequently, two main phase powders with an average particle size of about 3.8 μm were obtained through hydrogen explosion and jet milling processes.
[0063] (2) Preparation of low melting point heavy rare earth grain boundary reconstruction alloy
[0064] According to the phase diagram of the alloy and the mixing enthalpy between elements, the alloy composition is designed to reconstruct the grain boundary of heavy rare earth elements with low melting point. around th...
Embodiment 3
[0070] This embodiment includes the following steps.
[0071] (1) Preparation of Nd-Fe-B main phase powder with low rare earth content and NdFeB main phase powder containing high abundance rare earth
[0072] First prepare the Nd-Fe-B main phase powder with low rare earth content, and the NdFeB main phase powder containing high-abundance rare earth (the composition is Nd 12.3 Fe bal B 6.1 and (Nd 9.3 La 3.0 )Fe bal B 3.1 ). NdFeB quick-setting flakes are prepared by smelting and flake rapid cooling. Subsequently, two main phase powders with an average particle size of about 3.8 μm were obtained by hydrogen explosion and jet milling processes.
[0073] (2) Preparation of low melting point heavy rare earth grain boundary reconstruction alloy
[0074] According to the alloy phase diagram and inter-element mixing enthalpy, design the low-melting point heavy rare earth grain boundary to reconstruct the alloy composition. It is required that the alloy contains more heavy ra...
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