Environment-friendly flame-retardant single-component silane-modified polyether sealant and preparation method thereof
A silane-modified polyether, one-component technology, applied in the direction of polyether adhesives, chemical instruments and methods, adhesives, etc., can solve the problems of slow degradation, food pollution, etc., and achieve good product performance and environmental friendliness Effect
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Embodiment 1
[0036] Add 30 parts of STP-E10, 15 parts of diisononyl cyclohexane 1,2-dicarboxylate, 40 parts of aluminum hydroxide, 8.6 parts of nano-calcium carbonate, 0.2 parts of Tinuvin326, 0.2 parts of Tinuvin770 into the stirring tank, vacuum Stir for 5 minutes, heat up to 100-110°C and stir for 2 hours, then cool down to below 50°C under vacuum protection, add 1 part of vinyltrimethoxysilane, 2 parts of γ-aminopropyltrimethoxysilane, 0.5 parts of γ-glycidyl ether Oxypropyltrimethoxysilane, vacuum stirring for 30min, that is, a uniformly dispersed sealant.
Embodiment 2
[0038] 17 parts of STP-E10, 10 parts of cyclohexane 1,2-diisononyl dicarboxylate, 40 parts of aluminum hydroxide, 20 parts of melamine cyanurate, 9.8 parts of nano calcium carbonate, 0.20 parts of Tinuvin326, 0.20 parts Add Tinuvin770 into the stirred tank, stir in vacuum for 5 minutes, raise the temperature to 100-110°C and stir for 2 hours, then cool down to below 50°C under vacuum protection, add 1 part of vinyltrimethoxysilane, 1 part of N-β-(aminoethyl) -γ-aminopropyltrimethoxysilane, 0.1 part of 2,4,6-tris(dimethylaminomethyl)phenol, stirred in vacuum for 30 minutes, and a uniformly dispersed sealant was obtained.
Embodiment 3
[0040]Add 20 parts of STP-E30, 10 parts of polypropylene glycol, 30 parts of aluminum hydroxide, 20 parts of magnesium hydroxide, 16.7 parts of melamine cyanurate, 0.20 parts of Tinuvin326, and 0.20 parts of Tinuvin770 into the stirring tank, stir in vacuum for 5 minutes, and heat up Stir at 100-110°C for 2 hours, vacuum protect and cool down to below 50°C, add 1 part of vinyltrimethoxysilane, 1 part of γ-aminopropyltrimethoxysilane, 0.1 part of 1,8-diazabicyclo Undec-7-ene, stirred in vacuum for 30 minutes, then a uniformly dispersed sealant can be obtained.
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