Kieselguhr modification-based PP melt-blown filter element and preparation method thereof
A melt-blown filter element and diatomite technology, which is applied in separation methods, chemical instruments and methods, filtration separation, etc., can solve problems such as breeding microorganisms, filtering liquid pollution, and restricting the development of PP filter elements.
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[0017] The invention provides a method for preparing a diatomite-based modified PP melt-blown filter element, comprising:
[0018] 1) spraying the polymer coating on the surface of diatomite, then drying, soaking in dilute sulfuric acid solution, and filtering to obtain activated diatomite;
[0019] 2) spray the silver nitrate solution and the hydrazine sulfate solution on the surface of the activated diatomite at the same time, and let it stand to prepare the silver-modified diatomite;
[0020] 3) decocting and filtering the Chinese herbal medicine in water to obtain the Chinese herbal medicine extract and the Chinese herbal medicine filter cake;
[0021] 4) In the presence of protective gas, place silver-modified diatomite at 240-255°C for calcination for 25-40 minutes, then place the calcined product in Chinese herbal medicine extract for impregnation and filtration to obtain Chinese herbal medicine-modified diatoms earth;
[0022] 5) PP (polypropylene), AES (acrylonitril...
Embodiment 1
[0041] 1) Polymer coating (containing polyvinyl alcohol, 1.2% by weight of p-aminophenol platinum, 0.7% by weight of palladium (II)-2-(5-bromo-2-pyridylazo)-5-diethylaminophenol ) is sprayed on the surface of diatomite, then dried at 125°C for 6h, placed in 50°C and 18% by weight of dilute sulfuric acid solution for 2h, filtered to obtain activated diatomite, wherein, diatomite, polymer The weight ratio of paint and dilute sulfuric acid solution is 100:4:200;
[0042] 2) Spray 5% by weight of silver nitrate solution and 2.5% by weight of hydrazine sulfate solution on the surface of activated diatomite at the same time, and let it stand at 30°C for 5h to prepare silver-modified diatomite, wherein activated diatomite, The weight ratio of silver nitrate solution and hydrazine sulfate solution is 100:7:12;
[0043] 3) Mix lemongrass, platycodon, aloe vera, lotus pod, fennel, Poria cocos bark, reed root, chicken vine, magnolia officinalis and water according to the weight of 100:2...
Embodiment 2
[0047] 1) Polymer coating (containing polyvinyl alcohol, 0.8% by weight of p-aminophenol platinum, 0.2% by weight of palladium (II)-2-(5-bromo-2-pyridylazo)-5-diethylaminophenol ) is sprayed on the surface of diatomite, then dried at 120°C for 5h, placed in 45°C and 15% by weight of dilute sulfuric acid solution, soaked for 1h, and filtered to obtain activated diatomite, wherein, diatomite, polymer The weight ratio of paint and dilute sulfuric acid solution is 100:3:150;
[0048] 2) Spray 4% by weight of silver nitrate solution and 2% by weight of hydrazine sulfate solution on the surface of activated diatomite at the same time, and let it stand at 25°C for 4h to obtain silver-modified diatomite, wherein activated diatomite, The weight ratio of silver nitrate solution and hydrazine sulfate solution is 100:5:10;
[0049] 3) Mix lemongrass, platycodon, aloe vera, lotus pod, fennel, Poria cocos bark, reed root, chicken vine, magnolia officinalis and water according to the weight...
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