Manufacturing method of moisture-absorbing and anti-static polypropylene fibers
A technology of polypropylene fiber and manufacturing method, which is applied in the manufacture of conductive/antistatic filaments, single-component polyolefin rayon, rayon, etc., and can solve the problems of airtightness, easy dust absorption, and non-hygroscopicity.
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Embodiment 1
[0033] Embodiment 1: a kind of manufacture method of hygroscopic antistatic polypropylene fiber adopts following steps:
[0034] A) According to the number of parts by mass, take 0.8 parts of halloysite nanotubes whose characteristic parameters are 40nm in diameter and 500nm in length, 0.5 parts of laurylamine polyoxyethylene ether, 1.2 parts of nano-scale conductive mica powder, and 1.2 parts of characteristic parameters whose length is 0.5 μm, 0.01μm wide attapulgite rod crystals, 4.0 parts of 30% sodium bicarbonate aqueous solution by mass fraction, 0.2 parts of nanoscale calamine powder mixed, stirred in a superheated steam reactor at 150 °C, steamed for 45 minutes, and heated at 400 °C Vacuum microwave irradiation for 2 hours, then immerse in 80 parts of sulfamic acid solution with a mass fraction of 30% for vacuum moisture absorption treatment, after absorption, heat to 60°C for ultrasonic dispersion for 0.5 hours, then stir and disperse for 3.5 hours to obtain suspended ...
Embodiment 2
[0038] Embodiment 2: a kind of manufacture method of hygroscopic antistatic polypropylene fiber adopts following steps:
[0039] A) According to the number of parts by mass, take 1.0 parts of halloysite nanotubes with a characteristic parameter diameter of 70nm and a length of 1200nm, 0.75 parts of laurylamine polyoxyethylene ether, 1.6 parts of nano-scale conductive mica powder, and 1.4 parts of a characteristic parameter with a length of 2.5 μm, 0.05μm wide attapulgite rod crystal, 5.0 parts by mass fraction of 30% sodium bicarbonate aqueous solution, 0.45 parts of nano-scale calamine powder mixed, stirred in a superheated steam reactor at 160 ° C, steamed for 50 minutes, and then heated at 450 ° C Vacuum microwave irradiation for 3 hours, then immerse in 100 parts of sulfamic acid solution with a mass fraction of 30% for vacuum moisture absorption treatment, after absorption, heat to 75°C for ultrasonic dispersion for 1 hour, then stir and disperse for 4 hours to obtain susp...
Embodiment 3
[0043] Embodiment 3: a kind of manufacture method of hygroscopic antistatic polypropylene fiber, adopts following steps:
[0044] A) According to the number of parts by mass, take 1.2 parts of halloysite nanotubes whose characteristic parameters are 100nm in diameter and 2000nm in length, 1.0 parts of laurylamine polyoxyethylene ether, 2.0 parts of nano-scale conductive mica powder, and 1.6 parts of characteristic parameters whose length is 5 μm , with a width of 0.10 μm attapulgite rod crystals, 6.0 parts by mass fraction of 30% sodium bicarbonate aqueous solution, and 0.7 parts of nano-scale calamine powder are mixed, stirred in a superheated steam reactor at 170 ° C, and after steaming for 60 minutes, vacuum at 500 ° C Microwave irradiated for 4 hours, then immersed in 120 parts of sulfamic acid solution with a mass fraction of 30% for vacuum moisture absorption treatment, heated to 95°C for 1.5 hours with ultrasonic dispersion after absorption, and then stirred and disperse...
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Abstract
Description
Claims
Application Information
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