Adhesive layer and adhesive film
An adhesive layer and adhesive technology, applied in the directions of adhesives, adhesive types, ester copolymer adhesives, etc., can solve the problems of reduced yield, difficulty in improving screen display performance, and inability to be practical, and achieve the purpose of maintaining the surface. The effect of hardness
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Embodiment 1
[0058] Introduce nitrogen gas into the reaction device equipped with a stirrer, thermometer, reflux cooler and nitrogen gas introduction pipe, and replace the air in the reaction device with nitrogen gas. After that, 75 parts by weight of butyl acrylate, 25 parts by weight of tert-butyl acrylate, 1.0 part by weight of 8-hydroxyoctyl acrylate, and 60 parts by weight of a solvent (ethyl acetate) were added to the reaction device. Thereafter, 0.1 parts by weight of azobisisobutyronitrile as a polymerization initiator was dripped over 2 hours, and reacted at 65° C. for 6 hours to obtain an acrylic polymer solution used in Example 1.
Embodiment 2~5 and comparative example 1~3
[0060] In the same manner as the acrylic polymer solution 1 used in Example 1 above, except that the composition of the monomers was set as described in Group (1) and Group (2) of Table 1, the 2-5 and the acrylic polymer solutions of Comparative Examples 1-3.
[0061]
[0062] [Example 1]
[0063] For the acrylic polymer solution of Example 1 prepared as described above, add 0.2 parts by weight of CORONATE HX (isocyanurate body of HDI), 0.05 parts by weight of KBM-803 (3-mercaptopropyltrimethoxysilane) , stirring and mixing to obtain the adhesive composition of Example 1. After coating this adhesive composition on a release film (polyethylene terephthalate (PET) film coated with a silicone resin), the solvent was removed by drying at 90°C, and then dried at 23°C , 50% RH atmosphere for 7 days, thereby obtaining the adhesive film of Example 1 having an adhesive layer crosslinked through the adhesive composition on one side of the release film.
[0064] [Examples 2-5 and Co...
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