Heat conducting pouring sealant material and preparation method thereof
A heat-conducting potting and heat-conducting powder technology, applied in the direction of adhesives, adhesive additives, non-polymer adhesive additives, etc., can solve the problems of insufficient thermal conductivity and insufficient density, and achieve low density and good thermal conductivity Effect
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[0049] The preparation method of the heat-conducting potting adhesive material of the present invention is formed by mixing various raw materials.
[0050] In the above preparation method, the mixing method can be implemented by using a high-speed disperser or a planetary stirring device. Specifically, the rotational speed of mixing by a high-speed disperser can be controlled at 800-3000 rpm, and the mixing time is 30-100 minutes. The speed of mixing with planetary mixing equipment can be controlled at 30-80rpm, and the mixing time is 30-100min.
[0051] In the mixing step, the product can also be vacuum defoamed.
Embodiment 1
[0053] First, the ratio of raw materials. Specifically: 50g of a mixture composed of vinyl silicone oil and hydrogen-containing silicone oil, 50g of vinyl silicone oil, 100g of alumina powder (D 50 35μm), 3g airgel, 0.2g coupling agent, 30g flame retardant.
[0054] Both the alumina powder and the airgel are dried, and then the surface is treated with a coupling agent according to a conventional method. Then, the aluminum oxide powder and the airgel are respectively added into the silicone polymer, stirred in a double planetary mixer for 50-60 minutes, and vacuum degassed to form A component and B component. Finally, mix A / B component 1:1 evenly, pour into the mold, and solidify at room temperature or heat.
Embodiment 2
[0056] First, the ratio of raw materials. Specifically: 50g of a mixture composed of vinyl silicone oil and hydrogen-containing silicone oil, 50g of vinyl silicone oil, 100g of alumina powder (D 50 35μm), 3g glass beads (D 50 65μm), 0.2g coupling agent, 30g flame retardant.
[0057] Both the alumina powder and the airgel are dried, and then the surface is treated with a coupling agent according to a conventional method. Then, the aluminum oxide powder and the airgel are respectively added into the silicone polymer, stirred in a double planetary mixer for 50-60 minutes, and vacuum degassed to form A component and B component. Finally, mix A / B component 1:1 evenly, pour into the mold, and solidify at room temperature or heat.
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