Alumina bioceramics material and preparation method therefor

A bio-ceramic material and alumina technology are applied in the field of alumina bio-ceramic materials and their preparation, which can solve the problems of limited service life and life of alumina ceramic materials, and achieve the effects of high compressive strength and hardness, and simple preparation process.

Inactive Publication Date: 2016-09-21
SUZHOU COSMETIC MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But like other ceramic materials, this ceramic has the inherent fatal weakness of brittleness, which limits the range of use and life of alumina ceramic materials considerably.

Method used

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  • Alumina bioceramics material and preparation method therefor

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Step 1: 28 parts of aluminum oxide, 3 parts of molybdenum boride, 5 parts of boron nitride, 2 parts of chromium boride, 3 parts of tungsten silicide, 4 parts of cobalt silicide, 4 parts of magnesium oxide, 2 parts of copper, 3 parts of zirconium, 2 parts of rubidium, and 3 parts of nickel are mechanically ball milled in a ball mill, the ball-to-material ratio in the ball mill is 30:1, and the ball milling time is 2 hours;

[0039] Step 2: After ball milling, mix the mixed cermet material evenly;

[0040] Step 3: Sinter the mixture evenly mixed in step (2) in a high-temperature sintering furnace at a temperature of 900°C for 3 hours, then increase the temperature to 1050°C, sinter for 4 hours, and cool to room temperature to prepare alumina bioceramic materials.

Embodiment 2

[0042] Step 1: 16 parts of aluminum oxide, 6 parts of molybdenum boride, 3 parts of boron nitride, 5 parts of chromium boride, 7 parts of tungsten silicide, 8 parts of cobalt silicide, 2 parts of magnesium oxide, 4 parts of copper, 1 part of zirconium, 5 parts of rubidium, and 1 part of nickel are mechanically ball milled in a ball mill, the ball-to-material ratio in the ball mill is 20:1, and the ball milling time is 4 hours;

[0043] Step 2: After ball milling, mix the mixed cermet material evenly;

[0044] Step 3: Sinter the mixture evenly mixed in step (2) at high temperature in a high-temperature sintering furnace, sinter at a temperature of 800°C for 3 hours, then increase the temperature to 950°C, sinter for 4 hours, and cool to room temperature to prepare alumina bioceramic materials.

Embodiment 3

[0046] Step 1: 20 parts of aluminum oxide, 5 parts of molybdenum boride, 3 parts of boron nitride, 3 parts of chromium boride, 6 parts of tungsten silicide, 5 parts of cobalt silicide, 4 parts of magnesium oxide, 3 parts of copper, 1 part of zirconium, 4 parts of rubidium, and 3 parts of nickel are mechanically ball milled in a ball mill. The ball-to-material ratio in the ball mill is 20:1, and the ball milling time is 4 hours;

[0047] Step 2: After ball milling, mix the mixed cermet material evenly;

[0048] Step 3: Sinter the mixture evenly mixed in step (2) in a high-temperature sintering furnace at a temperature of 900°C for 3 hours, then increase the temperature to 1050°C, sinter for 4 hours, and cool to room temperature to prepare alumina bioceramic materials.

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Abstract

The invention belongs to the field of medical materials and discloses an alumina bioceramics material and a preparation method therefor. The ceramic material is prepared from the ingredients in parts by weight: 16-28 parts of alumina, 3-6 parts of molybdenum boride, 3-5 parts of boron nitride, 2-5 parts of chromium boride, 3-7 parts of tungsten silicide, 4-8 parts of cobalt silicide, 2-4 parts of magnesia, 2-4 parts of copper, 1-3 parts of zirconium, 2-5 parts of rubidium and 1-3 parts of nickel. The preparation method disclosed by the invention comprises the following steps: (1) carrying out mechanical ball-milling on the ingredients (in parts by weight) in a ball mill; (2) after ball-milling, uniformly mixing a mixed cermet material; and (3) carrying out high-temperature sintering on the mixture, which is uniformly mixed in the step (2), in a high-temperature sintering furnace for 3 hours at the temperature of 800 DEG C to 900 DEG C, then, heating the mixture to the temperature of 950 DEG C to 1,050 DEG C, carrying out sintering for 4 hours, and cooling the mixture to room temperature, thereby preparing the alumina bioceramics material.

Description

technical field [0001] The invention belongs to the field of new biological materials, and relates to an alumina bioceramic material and a preparation method thereof. Background technique [0002] With the development of science and technology and the improvement of manufacturing technology, alumina ceramics have been more and more widely used in modern industry and modern science and technology. For example, in terms of machinery, there are wear-resistant alumina ceramic lining bricks, lining plates, linings, alumina ceramic nails, ceramic seals, black alumina ceramic cutting tools, red alumina ceramic plungers, etc. In terms of electronics and electricity, there are various alumina ceramic bottom plates, substrates, ceramic membranes, transparent alumina ceramics for high-pressure sodium lamps, and various alumina ceramic electrical insulating porcelain parts, electronic materials, and magnetic materials. In medicine, there are alumina ceramic artificial bones, hydroxyapa...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/10
CPCC04B35/10C04B2235/3206C04B2235/3804C04B2235/386C04B2235/3891C04B2235/40C04B2235/405C04B2235/407C04B2235/96
Inventor 尤志刚
Owner SUZHOU COSMETIC MATERIALS
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