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Medicinal toothpaste containing nutgall ethyl acetate extract and production method thereof

A technology of seed ethyl acetate and production method, which is applied in the fields of pharmaceutical formula, dentistry, medical science, etc., can solve the problems of being easily oxidized, precipitated, etc., and achieve the effect of increasing service life and frequency, and improving stability

Inactive Publication Date: 2016-05-04
SHIHEZI UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are a large number of adjacent phenolic hydroxyl groups in the structure of gallic tannins, which are easily oxidized. During the shelf life of some sipayi gum gels, there will be visible precipitation at the bottom of the bottle. Improving the stability of gallic tannins is also the reason for sipayi collapsing. One of the difficulties that researchers face

Method used

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  • Medicinal toothpaste containing nutgall ethyl acetate extract and production method thereof
  • Medicinal toothpaste containing nutgall ethyl acetate extract and production method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0027] Step 1: Soak the galls in petroleum ether and percolate, recover the residue, evaporate the petroleum ether in the residue, and then extract it with deionized water under reflux. After the extract is concentrated, it is extracted with ethyl acetate of the same volume as the concentrated solution, and the upper layer is collected The clear liquid was evaporated to dryness to obtain the ethyl acetate extract.

[0028] The second step: take 10 parts of silicon dioxide, 25 parts of calcium carbonate, 2 parts of sodium lauryl sulfate, 15 parts of glycerin, 15 parts of sorbitol, 1.5 parts of sodium carboxymethyl cellulose, 0.6 parts of sodium saccharin, flavor 1.4 spares.

[0029] The third step: making ointment, first disperse 1.5 parts of sodium carboxymethylcellulose evenly in 15 parts of glycerol and 15 parts of sorbitol, and then dissolve 0.6 parts of sodium saccharin and 0.4 parts of sodium nitrate in 15 parts of purified water part, mix the two solutions under stirrin...

Embodiment 2

[0031] Step 1: Soak the galls in petroleum ether and percolate, recover the residue, evaporate the petroleum ether in the residue, and then extract it with deionized water under reflux. After the extract is concentrated, it is extracted with ethyl acetate of the same volume as the concentrated solution, and the upper layer is collected The clear liquid was evaporated to dryness to obtain the ethyl acetate extract.

[0032] Step 2: Take 30 parts of silicon dioxide, 2.2 parts of sodium lauryl sulfate, 10 parts of glycerin, 20 parts of sorbitol, 0.5 parts of sodium carboxymethylcellulose, 0.3 parts of sodium saccharin, and 1.2 parts of essence for later use.

[0033] The third step: making ointment, first disperse 0.5 parts of sodium carboxymethylcellulose in 10 parts of glycerol and 20 parts of sorbitol, and then dissolve 0.3 parts of sodium saccharin and 0.3 parts of sodium nitrate in 15 parts of purified water , mix the two solutions under stirring to make it swell into a unif...

Embodiment 3

[0035] Step 1: Soak the galls in petroleum ether and percolate, recover the residue, evaporate the petroleum ether in the residue, and then extract it with deionized water under reflux. After the extract is concentrated, it is extracted with ethyl acetate of the same volume as the concentrated solution, and the upper layer is collected The clear liquid was evaporated to dryness to obtain the ethyl acetate extract.

[0036] Step 2: Take 20 parts of silicon dioxide, 10 parts of calcium carbonate, 3 parts of sodium lauryl sulfate, 30 parts of glycerin, 1.2 parts of sodium carboxymethyl cellulose, 0.5 parts of sodium saccharin, and 1.2 parts of essence for later use.

[0037] The third step: making ointment, first disperse 1.2 parts of sodium carboxymethylcellulose evenly in 30 parts of glycerol, and then dissolve 0.5 parts of sodium saccharin and 0.3 parts of sodium nitrate in 25 parts of purified water, and stir Mix the two solutions to make it swell into a uniform colloid, also...

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Abstract

The invention relates to medicinal toothpaste containing nutgall ethyl acetate extract and a production method thereof. The medicinal toothpaste provided by the invention contains the nutgall ethyl acetate extract, an abrasive, a foaming agent, a humectant, a thickening agent, a sweetening agent, a preservative, a corrosion inhibitor, essence and refined water. The production method of the medicinal toothpaste containing the nutgall ethyl acetate extract comprises the following steps: firstly, preparing nutgall ethyl acetate extract; secondly, taking the abrasive, foaming agent, humectant, thickening agent, preservative, corrosion inhibitor and sweetening agent for later use; and thirdly, preparing toothpaste by adopting a two-step process. The medicinal toothpaste provided by the invention has the advantages that nutgall active ingredient is added during production of the toothpaste, guarantee period of a product is prolonged and number of times of the product is increased, the toothpaste can have antibacterial and anti-inflammation effects, and besides cleaning teeth, the toothpaste also can be used for treating limp teeth, chewing disability, gingival bleeding, mouth and tongue sores, swelling and pain in throat, halitosis and the like which are caused by periodontal disease.

Description

technical field [0001] The invention relates to a Chinese herbal medicine toothpaste and a production method thereof, in particular to a medicine toothpaste containing gallic ethyl acetate extract and a production method thereof. Background technique [0002] Periodontitis is a common oral disease. Its prevalence rate is as high as 80% among adults in my country. The main symptoms are bleeding gums, red and swollen gums, and bad breath. This disease is mostly caused by the imbalance of oral bacteria. [0003] Xipayi Gingival Liquid is a classic prescription for oral health care in Uyghur medicine. It is prepared from a single herbal medicine called gallaceae. Types of storage. The complete preparation method recorded in the sub-volume of Uyghur medicine is: "Take 20g of gall, crush it into a coarse powder, add water to soak for 1 hour, decoct 3 times, each time for 0.5 hours, combine the decoction, filter, add 20g of cyclamate in turn to the filtrate , mint essence 1mL and...

Claims

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Application Information

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IPC IPC(8): A61K8/97A61Q11/00
CPCA61K8/97A61Q11/00
Inventor 韩博陈海君陈文于玮龙飞马尚智谢智勇姚美村屠鹏飞
Owner SHIHEZI UNIVERSITY
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