One-component RTV silicone sealing material for LED lamp and preparation method thereof
A technology of LED lamps and vulcanized silicone, applied in the directions of adhesive additives, non-polymer adhesive additives, polymer adhesive additives, etc. problems such as decline, to achieve the effect of excellent yellowing resistance, excellent adhesion, and improved adhesion
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Embodiment 1
[0034] A one-component room temperature vulcanizing silicone sealant for LED lamps, the raw materials of which are composed of:
[0035]
[0036] The preparation method of the above-mentioned one-component room temperature vulcanizing silicone sealant for LED lamps in this embodiment, the steps are as follows:
[0037] Add the α,ω-bis(trimethoxysiloxy)polydimethylsiloxane and the active nano-calcium carbonate whose surface has been treated with hard fatty acid or castor oil into the kneader. Stir for 2 hours under the condition of vacuum degree of -0.095MPa, remove the moisture in the raw material under high temperature vacuum, and cool to room temperature to obtain a base material with uniform appearance;
[0038] Add the prepared base material, long-chain methyl silicone oil, and a mixture of polymethyltrimethoxysilane and methyltrimethoxysilane to the planetary machine, stir and react for 0.5h under nitrogen protection, and then add colorless and transparent titanic acid...
Embodiment 2
[0040] A one-component room temperature vulcanizing silicone sealant for LED lamps, the raw materials of which are composed of:
[0041]
[0042] The preparation method of the above-mentioned one-component room temperature vulcanizing silicone sealant for LED lamps in this embodiment, the steps are as follows:
[0043] Add the α,ω-bis(trimethoxysiloxy)polydimethylsiloxane and the active nano-calcium carbonate whose surface has been treated with hard fatty acid or castor oil into the kneader. Stir for 2 hours under the condition of vacuum degree of -0.095MPa, remove the moisture in the raw material under high temperature vacuum, and cool to room temperature to obtain a base material with uniform appearance;
[0044] Add the prepared base material, long-chain methyl silicone oil, and a mixture of polymethyltrimethoxysilane and methyltrimethoxysilane to the planetary machine, stir and react for 0.5h under nitrogen protection, and then add colorless and transparent titanic acid...
Embodiment 3
[0046] A one-component room temperature vulcanizing silicone sealant for LED lamps, the raw materials of which are composed of:
[0047]
[0048] The preparation method of the above-mentioned one-component room temperature vulcanizing silicone sealant for LED lamps in this embodiment, the steps are as follows:
[0049] Add the α,ω-bis(trimethoxysiloxy)polydimethylsiloxane and the active nano-calcium carbonate whose surface has been treated with hard fatty acid or castor oil into the kneader. Stir for 2 hours under the condition of vacuum degree of -0.095MPa, remove the moisture in the raw material under high temperature vacuum, and cool to room temperature to obtain a base material with uniform appearance;
[0050] Add the prepared base material, long-chain methyl silicone oil, and a mixture of polymethyltrimethoxysilane and methyltrimethoxysilane to the planetary machine, stir and react for 0.5h under nitrogen protection, and then add colorless and transparent titanic acid...
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Abstract
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