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Novel composite coating of diamond applied to stone cutter

A stone cutting and composite coating technology, which is applied in metal material coating technology, coating, liquid chemical plating, etc., can solve the problems of weak bonding between the coating layer and diamond, limited atomic diffusion ability, and difficulty in meeting actual needs, etc. , to achieve the effect of easy large-scale production, low requirements for equipment and easy operation

Active Publication Date: 2015-12-23
SHANDONG JIANZHU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In order to obtain the ideal metal coating layer on the diamond surface, various methods can be used, such as the combination of chemical plating and electroplating, vacuum plating, salt bath plating, vacuum physical vapor plating and physical chemical vapor plating, etc., but these plating The method generally has problems such as uneven plating, weak bonding between the plating layer and the diamond, low single plating amount, difficulty in controlling the plating thickness, and high cost.
Among them, the vacuum micro-evaporation plating method developed by Yanshan University can realize the process of plating Ti as low as 650°C, but the atom diffusion ability is limited at low temperature, and the formed coating is thin, which is difficult to meet the actual needs.

Method used

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  • Novel composite coating of diamond applied to stone cutter
  • Novel composite coating of diamond applied to stone cutter
  • Novel composite coating of diamond applied to stone cutter

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] 1. Preparation of the solution: a. The preparation of the salt-based colloidal palladium solution is to dissolve 0.5g of palladium chloride in 40mL of concentrated hydrochloric acid, then add 16g / L of tin chloride therein, and get another 160g / L of chloride Sodium was dissolved in 1L of water, and the two solutions were mixed under constant stirring, and kept at 50°C for 3 hours to obtain a base colloidal palladium solution. b. The preparation process of the hydrothermal composite titanium plating and tungsten solution is: add the completely dissolved nickel sulfate into the complexing agent containing sodium citrate, lactic acid, diacid and tartaric acid solution under constant stirring, and dissolve an appropriate amount of Sodium tungstate; slowly add the completely dissolved reducing agent sodium dihydrogen phosphate into the aforementioned solution under vigorous stirring; add rare earth chloride and titanium powder, add stabilizer thiourea to dissolve, and adjust ...

Embodiment 2

[0028] Hydrothermal composite plating: Put the diamond obtained in step 2 of [Example 1] into the solution with pH=4.0 prepared in step 1 b, mix it ultrasonically, pour it into a reaction kettle, and keep it in a drying oven at 120°C for 6 hours. Other steps are identical with [embodiment 1], as figure 1 (b) shown. Its composition is distributed as figure 2 shown.

Embodiment 3

[0030] Hydrothermal composite plating: Put the diamond obtained in step 2 into the pH=4.0 prepared in step 1 b, mix it ultrasonically, pour it into the reaction kettle, and keep it in a drying oven at 130°C for 6 hours. Other steps are identical with [embodiment 1], as figure 1 (c) shown.

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Abstract

The invention provides a preparing technology of a surface hydrothermal composite titanizing and tungsten plating metal layer of the diamond applied to a stone cutter, and belongs to the technical field of diamond surface plating metal layer film preparing. The low-temperature pressure plating and high-temperature thermal treatment technology is achieved, the continuity and uniformity of an obtained film are good, the shape is regular, the thickness is controllable, the strength of the diamond is improved, and the anti-corrosion capability and bonding performance under the high temperature are improved. The service life of the manfuactured cutter during stone cutting is greatly prolonged, the efficiency of the manufactured cutter during stone cutting is greatly improved, and economic benefits are obvious. The preparing method is simple and low in cost, and large-scale production is easy to achieve. Thus, the technology method has very wide application prospects.

Description

technical field [0001] The invention belongs to the technical field of film preparation of metal layer coated on diamond surface, and in particular relates to a preparation process of hydrothermal composite titanium and tungsten metal layer coating on diamond surface. Background technique [0002] Diamond itself not only has excellent properties such as high hardness, corrosion resistance and wear resistance, but also has excellent optical, acoustic, thermal and electrical properties. For more than half a century, the production and application technology of artificial diamond has developed by leaps and bounds, and its quantity, quality and many properties have reached or even surpassed that of natural diamond. Diamond and its products are not only widely used in various industrial and technical fields such as machinery, metallurgy, construction, transportation, and national defense, but also have been expanded to important fields such as high-performance heat-resistant part...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C18/48C23C18/18
Inventor 项东石磊王志刚宋文婷史璐玉刘慧敏
Owner SHANDONG JIANZHU UNIV
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