A kind of coating preparation method of phosphoric acid microporous acidifying agent granules
A technology of acidifier and granular material, which is applied in the field of coating preparation of feed acidifier, which can solve the problems of acidifier strong irritation, volatile instability, and incomplete coating, so as to improve the intestinal environment and production environment , reduce artificial effects
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Embodiment 1
[0020] The specific steps of the coating preparation method of phosphoric acid microporous acidifier particles are as follows:
[0021] (1) Mix 10 parts of chitosan, 10 parts of citric acid, and 10 parts of malic acid through a 300-mesh sieve, add 20 parts of lactic acid and 5 parts of polyethylene glycol, and spray granulate after mixing evenly; air inlet for spray granulation The temperature is 90°C, the outlet temperature is 60°C, and the granulation size is 100 microns.
[0022] (2) Combine 3 parts of phosphoric acid, 1 part of formic acid, 8 parts of acetic acid, 3 parts of propionic acid, 8 parts of butyric acid, 10 parts of hydroxypropyl methylcellulose, 2 parts of fumed silica and the compound obtained in step (1). The pellets are evenly mixed and granulated by a screw extruder; the particle size of the screw extruder is 300 microns. During the granulation process, a symmetrical high-pressure nitrogen gas flow with a pressure of 0.15Mpa is relatively rushed toward the gran...
Embodiment 2
[0026] The specific steps of the coating preparation method of phosphoric acid microporous acidifier particles are as follows:
[0027] (1) Mix 12 parts of chitosan, 15 parts of citric acid, and 15 parts of malic acid through a 300-mesh sieve, add 30 parts of lactic acid and 8 parts of polyethylene glycol, mix evenly and spray granulation; the air inlet of spray granulation The temperature is 100°C, the outlet temperature is 70°C, and the granulation particle size is 150 microns.
[0028] (2) Combine 5 parts of phosphoric acid, 2 parts of formic acid, 10 parts of acetic acid, 5 parts of propionic acid, 10 parts of butyric acid, 12 parts of hydroxypropyl methylcellulose, 3 parts of fumed silica and the compound obtained in step (1). The pellets are evenly mixed and granulated by a screw extruder; the particle size of the screw extruder is 500 microns. During the granulation process, the left and right symmetrical high-pressure argon gas flow with a pressure of 0.18Mpa is relatively...
Embodiment 3
[0032] The specific steps of the coating preparation method of phosphoric acid microporous acidifier particles are as follows:
[0033] (1) Mix 11 parts of chitosan, 12 parts of citric acid, and 12 parts of malic acid through a 300-mesh sieve, add 25 parts of lactic acid and 7 parts of polyethylene glycol, mix well and spray granulation; the air inlet for spray granulation The temperature is 95°C, the outlet temperature is 65°C, and the granulation size is 120 microns.
[0034] (2) Combine 4 parts of phosphoric acid, 1.5 parts of formic acid, 9 parts of acetic acid, 4 parts of propionic acid, 9 parts of butyric acid, 11 parts of hydroxypropyl methylcellulose, 2.5 parts of fumed silica and the compound obtained in step (1). The pellets are evenly mixed and granulated by a screw extruder; the particle size of the screw extruder is 400 microns. During the granulation process, a symmetrical high-pressure nitrogen gas flow with a pressure of 0.16Mpa rushes towards the granulated materi...
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