An integrally formed ceramic heating body and its preparation process
A ceramic heating body, an integrated technology, applied in the field of preparation technology of ceramic heating body, can solve the problems of unstable product performance, easy short cracking of tungsten wire, low yield and other problems
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Embodiment 1
[0076] The preparation process of an integrally formed ceramic heating body in this embodiment includes the following process steps:
[0077] a. Mixing: first mix 70% Si by mass 3 N 4 , 9% MgO, 5% Y 2 o 3 , 5% Al 2 o 3 , 5% SiO 2 , 3% La 2 o 3 , 3% BN mixed and stirred evenly to make ceramic raw materials, and then 50% ceramic raw materials and 50% heating raw materials MoSi 2 Mix and stir evenly to make powder;
[0078] b. Ball milling: put the powder, grinding balls, water or alcohol prepared in step a into a ball milling tank for wet ball milling, and the time for wet ball milling is 8 hours;
[0079] c, filter and dry: carry out solid-liquid separation to the slurry after wet ball milling in step b, dry the powder after separation;
[0080] d. Hot die-casting molding: adding paraffin wax to the dried powder in step c, heating and stirring, stirring evenly to form a slurry, adding the slurry to a hot press for die-casting, and molding the powder to obtain a green ...
Embodiment 2
[0086] The preparation process of an integrally formed ceramic heating body in this embodiment includes the following process steps:
[0087] a, mixing: first mix Si with a mass percentage of 96% 3 N 4 , 1% MgO, 1% Y 2 o 3 , 0.5% Al 2 o 3 , 0.5% SiO 2 , 0.5% La 2 o 3 , 0.5% BN mixed and stirred evenly to make ceramic raw materials, and then 95% ceramic raw materials and 5% heating raw material TiC were mixed and stirred evenly to make powder;
[0088] b. Ball milling: put the powder, grinding balls, water or alcohol prepared in step a into a ball milling tank for wet ball milling, and the time for wet ball milling is 11 hours;
[0089] c, filter and dry: carry out solid-liquid separation to the slurry after wet ball milling in step b, dry the powder after separation;
[0090] d. Dry press forming: add the powder after drying in step c to a binder and mix and stir, mix evenly to form a powder, put the powder into a hydraulic press for dry press forming, and form the po...
Embodiment 3
[0096] The preparation process of an integrally formed ceramic heating body in this embodiment includes the following process steps:
[0097] a. Mixing: first mix Si with 80% mass percentage 3 N 4 , 6% MgO, 4% Y 2 o 3 , 4% Al 2 o 3 , 4% SiO 2 , 1% La 2 o 3 , 1% BN mixed and stirred evenly to make ceramic raw materials, and then 60% ceramic raw materials, 20% heating raw materials TiC, 20% heating raw materials MoSi 2 Mix and stir evenly to make powder;
[0098] b. Ball milling: put the powder, grinding balls, water or alcohol prepared in step a into a ball milling tank for wet ball milling, and the time for wet ball milling is 14 hours;
[0099] c, filter and dry: carry out solid-liquid separation to the slurry after wet ball milling in step b, dry the powder after separation;
[0100] d. Extrusion molding: add the powder after drying in step c to a binder and mix and stir, mix evenly to form a powder, put the powder into an extruder for extrusion molding, and mold t...
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