A kind of honeycomb low-temperature denitrification catalyst and preparation method thereof
A low-temperature denitrification and catalyst technology, applied in chemical instruments and methods, physical/chemical process catalysts, metal/metal oxide/metal hydroxide catalysts, etc., can solve the problem of high active temperature window, difficulty in catalyst preparation, and increased operating costs and other problems, to achieve high low-temperature activity, broaden the activity temperature window, and improve the effect of microscopic properties
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Embodiment 1
[0037] Example 1 Preparation of Catalyst C1.
[0038] Dissolve manganese acetate tetrahydrate, ferric nitrate nonahydrate, and cerium nitrate hexahydrate in 50ml deionized water to form a mixed solution, and add 20g of γ-Al to the solution 2 o 3 Powder, control the mass ratio of metal elements to carrier Mn:Fe:Ce:Al 2 o 3 =8:2:4:100. First, use a magnetic constant temperature stirrer to stir at a constant temperature of 40 ° C for 1 h, then put the sample into an ultrasonic generator for ultrasonic impregnation, the ultrasonic power is 300 W, the frequency is 30 Khz, and the impregnation time is 2 h. Then add 15g binder and make slurry, the composition of binder is: colloidal silicon dioxide 60wt%, polyvinyl alcohol 25wt% and carboxymethyl cellulose 15wt%. After stirring, put the cordierite ceramic honeycomb carrier into the slurry and impregnate it with the above ultrasonic parameters for 5 hours, then put the impregnated cordierite ceramic honeycomb carrier into a microw...
Embodiment 2
[0039] Example 2 Preparation of Catalyst C2.
[0040] The implementation steps are the same as in Example 1, other conditions remain unchanged, and the mass ratio of Mn:Fe:Ce is changed to 8:2:6 to prepare catalyst C2.
Embodiment 3
[0041] Example 3 Preparation of Catalyst C3.
[0042] The implementation steps are the same as in Example 1, other conditions remain unchanged, and the mass ratio of Mn:Fe:Ce is changed to 8:4:6 to prepare catalyst C3.
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