Method for determining cadmium and trace lead in iron ore
An iron ore and micro-quantity technology, applied in the field of physical and chemical testing, can solve the problems of expensive ICP-MS method, difficulty in popularizing testing companies, and insufficient sensitivity to meet the requirements, and achieve rapid sample decomposition, low loss, and low reagent consumption. Effect
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[0022] 1.1 Main Instruments
[0023] AA240Z graphite furnace atomic absorption spectrometer (Varian, USA); PSD120 graphite furnace autosampler (Varian, USA); O2E-05 cadmium hollow cathode lamp; WB24A lead hollow cathode lamp. ETHOS A microwave digestion instrument (LabTech, USA), equipped with 12 100mL high-pressure digestion tanks. Milli-Q Advantage A10 ultrapure water system (Millipore, USA): resistivity 18.2MΩ·cm.
[0024] 1.2 Main reagents
[0025] Lead and cadmium standard stock solutions (National Iron and Steel Materials Testing Center): Both are 1000 μg / mL, diluted into standard working solutions of different concentrations as required (see Table 1).
[0026] Table 1 Concentrations of Pb and Cd in standard working solutions
[0027]
[0028] 1.3 Experimental method
[0029] Weigh 0.5g iron ore sample dried at 105°C, place it in a 100mL polytetrafluoroethylene digestion tank, moisten it with a small amount of deionized water, add 10mL aqua regia, and wait for the...
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