Non-aqueous solvent composition with temperature control separation performance for active dye
A technology of reactive dyes and non-aqueous solvents, applied in the field of textile dyeing and finishing, can solve the problems of rising water costs and other issues, and achieve the effects of saving energy consumption, reducing dyeing costs, and saving cycle time
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Embodiment 1
[0023] This embodiment provides a non-aqueous solvent composition with temperature-controlled separation performance for reactive dyes, which includes dimethyl sulfoxide and tetrachloroethylene, wherein the volume ratio of the two is 15:60.
[0024] Present embodiment also provides a kind of dyeing method of reactive dye, it comprises the following steps:
[0025] Mix the knitted fabric with an aqueous solution of sodium carbonate with a concentration of 20g / L for swelling, and control the liquid retention rate to 100%;
[0026] Put 2g of the pretreated knitted fabric into the dyeing cup, add 0.06g (3% o.m.f) of Avitera Red SE and 15mL of dimethyl sulfoxide, dye at 60°C, and adjust the heating rate to 1°C / min To 90°C, add a total of 60mL tetrachlorethylene in three batches during the heating process;
[0027] Incubate at 90°C for 1 hour, wring out the solvent from the cloth sample, and wash with water at room temperature to complete the dyeing.
[0028] Pour out the solvent,...
Embodiment 2
[0032] This embodiment provides a non-aqueous solvent composition with temperature-controlled separation performance for reactive dyes, which includes N,N-dimethylacetamide and n-hexane, wherein the volume ratio of the two is 15:75.
[0033] Present embodiment also provides a kind of dyeing method of reactive dye, it comprises the following steps:
[0034] Mix the knitted fabric with an aqueous solution of sodium carbonate with a concentration of 20g / L for swelling, and control the liquid retention rate to 100%;
[0035] Put 2g of the pretreated knitted fabric into the dyeing cup, add 0.06g (3% o.m.f) of Avitera Orange SE and 15mL of N,N-dimethylacetamide, dye at 60°C, and adjust the heating rate to 1 ℃ / min to raise the temperature to 90°C, and add 75mL of n-hexane in three batches during the heating process;
[0036] Incubate at 90°C for 1 hour, wring out the solvent from the cloth sample, and wash with water at room temperature to complete the dyeing.
[0037] Pour out the...
Embodiment 3
[0041] This embodiment provides a non-aqueous solvent composition with temperature-controlled separation performance for reactive dyes, which includes N,N-dimethylformamide and decamethylcyclopentasiloxane, wherein the volume of the two The ratio is 15:75.
[0042] Present embodiment also provides a kind of dyeing method of reactive dye, it comprises the following steps:
[0043] Mix the knitted fabric with an aqueous solution of sodium hydroxide with a concentration of 10g / L for swelling, and control the liquid retention rate to 100%;
[0044] Put 2g of the pretreated knitted fabric into the dyeing cup, add 0.06g (3% o.m.f) of Novacron Super Black G and 15mL of N,N-dimethylformamide, dye at 60°C, and adjust the heating rate to Raise the temperature to 95°C at 1°C / min, and add 75mL of n-hexane in three batches during the heating process;
[0045] Incubate at 90°C for 1 hour, wring out the solvent from the cloth sample, and wash with water at room temperature to complete the ...
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