Preparation method and application of graphene oxide liquid crystal emulsion
A technology of liquid crystal emulsion and graphene solution, which is applied in the direction of separation method and dispersed particle separation, can solve the problems of affecting experimental results, occurrence of deposition phenomenon, low material utilization rate, etc., and achieves large adsorption capacity, high energy density and strong desalination effect of ability
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[0028] Below by example the present invention will be further described
[0029] With 2g natural flake graphite as raw material, add 2g NaNO 3 , 92mL 98% concentrated H 2 SO 4 , 2g KMnO 4 , 560mL distilled water and 12mL 30% H 2 o 2 solution to prepare a graphene oxide dispersion; centrifuge at a speed of 9000 rpm, and when the pH value of the supernatant in the centrifuge tube is close to neutral, it indicates that the impurities in the graphene oxide solution have been removed. Take the slurry at the bottom of a 10mL centrifuge tube for freeze-drying, weigh the dried graphene oxide to obtain a mass of about 90mg, add deionized water to dilute it to 3mg / mL; take 40mL of a 3mg / mL graphene oxide solution, add 120mg D as surfactant and crosslinking agent 400 , after stirring for 20 minutes, add 60 mg of carbon black, stir evenly, then add 20 mL of vegetable oil, and emulsify it by ultrasonic to prepare a stable graphene oxide liquid crystal emulsion. Add 30 mL of deionize...
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