A kind of preparation method of copper/phosphorus bimetallic capillary
A technology of capillary and bimetal, which is applied in the field of metal composite capillary material preparation, can solve the problems of lowering the reliability of the instrument, shortening the service life, and low thermal conductivity of phosphorus, and achieves low production cost, long mold life and good surface quality Effect
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Embodiment 1
[0016] Embodiment 1: A processing method for a copper / phosphorus bimetallic capillary with a size of Φ3.0 mm×1.5 mm.
[0017] Put a TA2 pure phosphorus tube with a size of Φ12.7mm×1.55mm into a T2 copper tube with a size of Φ19.0mm×2.0mm, insert a mandrel coated with mineral oil, and perform 3 passes with a section reduction rate of about 20%. Cold swaging to produce a copper / phosphorus composite pipe with a size of Φ14.1mm×1.3mm. Under the protection of argon, the composite tube was subjected to diffusion annealing treatment at 950°C for 10 minutes to form a metallurgical bond at the interface. After the diffusion treatment, the composite pipe was subjected to 5 passes of straight pulling with the moving core to obtain a Φ7.2mm×0.7mm composite pipe, and after annealing at 500°C for 1h, the moving core was pulled continuously for 5 passes to obtain a Φ3. 0mm×1.5mm copper / phosphorus bimetallic capillary. The section reduction rate of the straight pull pass is between 10% and ...
Embodiment 2
[0018] Embodiment 2: A processing method for a copper / phosphorus alloy bimetallic capillary with a size of Φ2.0mm×0.4mm.
[0019] Put the phosphorus alloy tube with the size of Φ12.0mm×1.5mm into the T2 copper tube with the size of Φ15.0mm×1.4mm, insert the mandrel coated with mineral oil, and carry out 4 passes of cooling with the section reduction rate of about 20%. Swivel forging to produce a copper / phosphorus alloy composite tube with a size of Φ11.0mm×1.0mm. Under the protection of argon, the composite tube was subjected to diffusion annealing at 920°C for 30 minutes to form a metallurgical bond at the interface. After the diffusion treatment, the composite pipe is straight-drawn by the moving core head for 5 times to obtain a composite pipe of Φ5.5mm×1.5mm, annealed at 500°C for 1 hour, and then pulled by the moving core head for 5 times to obtain a composite pipe of Φ2mm. ×0.4mm copper / phosphorus alloy bimetallic capillary. The section reduction rate of the straight p...
Embodiment 3
[0020] Embodiment 3: A processing method for a copper / phosphorus bimetallic capillary with a size of Φ1.5 mm×0.1 mm.
[0021] Put a TA2 pure phosphorus tube with a size of Φ8.0mm×0.4mm into a T2 copper tube with a size of Φ10.0mm×0.9mm, insert a mandrel coated with mineral oil and perform 5 passes with a section reduction rate of about 20%. Cold swaging to produce a copper / phosphorus composite pipe with a size of Φ9.0mm×0.6mm. Under the protection of argon, the composite pipe was subjected to diffusion annealing treatment at 900°C for 60 minutes to form a metallurgical bond at the interface. After the diffusion treatment, the composite pipe is pulled by the moving core head 4 times to obtain a Φ4.0mm×0.3mm composite pipe; after annealing at 500°C for 1h, the Φ2 .0mm×0.15mm composite tube; after annealing at 500°C for 1h, it will be drawn into a Φ1.5mm×0.1mm copper / phosphorus bimetallic capillary through 7 passes (an intermediary at 500°C for 1h is required during this period)...
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