Preparation method of wear-resistant and flame-retardant swash plate
The technology of swash plate and wear-resistant coating is applied in the field of preparation of swash plate of automobile air-conditioning compressor, which can solve the problems of increasing the difficulty of preparation, harmful to social environment, increasing social energy consumption, etc., and achieves simple and controllable preparation process and reasonable composition. , The effect of easy adjustment of spray thickness
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Synthetic example 1
[0033] Synthesis Example 1 Synthesis of Silicon-containing Phosphate
[0034] Add 15mL trimethylbromosilane, 5ml diethanolamine, 30ml absolute ethanol and 2g potassium silanolate to the three-necked flask, reflux and stir for 5 hours, cool, and filter to obtain the liquid; add 2.5ml, 50ml of 85% phosphoric acid to the liquid Acetone and 1.2g of phosphorus pentoxide were heated to 60°C, stirred and reacted for 2 hours, the acetone was removed by distillation, and the obtained liquid was silicon-containing phosphate.
Synthetic example 2
[0035] Synthesis Example 2 Preparation of Composite Filler
[0036] Mix 380g of molybdenum disulfide and 100g of aluminum phosphate evenly, sinter at 500°C for 55min, and crush it into a powder with a particle size of 15-22μm, which is the composite filler.
Embodiment 1
[0038] A wear-resistant and flame-retardant swash plate, the preparation of which comprises the following steps:
[0039] (1) Preparation of Component A: In a nitrogen atmosphere, mix bisphenol A epoxy resin, maleic anhydride and ethylene glycol, react at 110° C. for 35 minutes, then add 5 drops of sulfuric acid with a concentration of 30%, and continue the reaction for 7 minutes Obtain an epoxy compound; then react the epoxy compound with bisphenol A cyanate at 150°C for 15 minutes to obtain Component A; wherein bisphenol A epoxy resin, maleic anhydride, ethylene glycol and bisphenol A cyanide The mass ratio of acid ester is 0.4: 1: 1.5: 1.5;
[0040](2) preparation of wear-resistant coating: dissolving component A in acetone to obtain mass concentration is the acetone solution of component A of 30%; then silicon-containing phosphate, PTFE particles, fluorinated graphite and composite filler are mixed uniformly, A solid lubricant is obtained; finally, the acetone solution of...
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