Antiglare film, method for producing same, polarizing plate, image display device, member for touch panel
A manufacturing method and technology of an anti-glare film, applied in polarizing elements, optical elements, diffusing elements, etc., can solve problems such as deterioration of visibility, darkening of the screen of a display device, and reduction of contrast
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Embodiment 1
[0385]
[0386] (Preparation of silica dispersion)
[0387] AEROSIL R812 (manufactured by Japan AEROSIL Co., Ltd., the average particle diameter of primary particles is 7nm)
[0388] 10 parts by mass
[0389] 90 parts by mass of ethanol
[0390] The above materials were stirred and mixed with a dissolver for 30 minutes, and then dispersed with a high-pressure homogenizer (Manton Gaulin). While stirring, 88 parts by mass of methylene chloride was added to the silica dispersion, and stirred and mixed in a dissolver for 30 minutes to prepare a silica dispersion dilution. Filtration was performed with a fine particle dispersion diluent filter (Advantec Toyo Co., Ltd.: POLYPROPYLENE WOUND CARTRIDGE FILTER) TCW-PPS-1N.
[0391]
[0392] (mucilage composition)
[0393] 90 parts by mass of cellulose triacetate
[0394] (Mn=148000, Mw=310000 acetyl substitution degree 2.92)
[0395] Aromatic terminal ester plasticizer (2-4) 10 pa...
Embodiment 2
[0595]
[0596] Using a micro-gravure coater, apply the following transparent hard coat coating composition 1 filtered through a polypropylene filter with a pore size of 0.4 μm on the base material film 1 produced in Example 1, and dry it in the constant-rate drying section. After drying at a temperature of 80°C and a deceleration drying zone temperature of 80°C, nitrogen purging is performed to obtain an atmosphere with an oxygen concentration of 1.0% by volume or less, while an ultraviolet lamp is used with an illuminance of 100mW / cm in the irradiated part 2 , irradiation dose 0.25J / cm 2 The coating layer was cured to form a transparent hard coat layer with a dry film thickness of 5 μm.
[0597] After the clear hard coat layer was formed, it was rolled into a roll to produce the clear hard coat film 1 . When the total haze of the clear hard coat film 1 was measured using a measuring machine (NDH2000) manufactured by Nippon Denshoku Industries Co., Ltd., it was 0.3%, and t...
Embodiment 3
[0639]
[0640] In preparation of the anti-glare film 1, the double-sided anti-glare film 1 was produced similarly except having provided the anti-glare layer coating layer composition 1 on both surfaces.
[0641] Next, a transparent conductive film of indium tin oxide (ITO) with a surface resistivity of about 200Ω was deposited on one side of the anti-glare layer by sputtering to produce Figure 7 Anti-glare film 1 with conductive film shown.
[0642]
[0643] In preparation of the anti-glare films 2-11, the double-sided anti-glare films 2-11 were produced similarly except having provided the anti-glare layer on both surfaces in the same manner as the double-sided anti-glare film 1.
[0644] Next, in the same manner as the preparation of the anti-glare film 1 with a conductive film, the anti-glare layer is coated on both sides, and the transparent conductive layer of ITO with a surface resistivity of about 200Ω is provided on one side of the anti-glare layer by sputtering...
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