High temperature and anti-composite salt polymer fluid loss reducer for drilling fluid and preparation method thereof
A fluid loss reducer and high temperature resistant technology, applied in drilling compositions, chemical instruments and methods, etc., can solve the problems of poor salt resistance and high temperature resistance, and achieve good salt and calcium resistance and good temperature resistance. , the effect of good lubricating performance
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Embodiment 1
[0027] 1.1 A fluid loss reducing agent for high temperature and compound salt polymers for drilling fluids, which consists of the following raw materials in percentage by weight: 12.2% acrylic acid, 7.2% sodium hydroxide, 62.3% deionized water, 5.5% acrylamide, four Sodium styrene sulfonate 5.5%, N-vinylpyrrolidone 7%, initiator 0.3%.
[0028] Prepare 1000kg of water loss reducing agent for high temperature and compound salt polymer used in drilling fluid of the present invention, specific raw materials and consumption are: 122kg of acrylic acid, 72kg of sodium hydroxide, 623kg of deionized water, 55kg of acrylamide, tetraphenylethylene sulfonic acid 55kg of sodium, 7kg of N-vinylpyrrolidone, and 3kg of initiator, wherein the initiator is 1.5kg of ammonium persulfate and 1.5kg of sodium sulfite.
[0029] 1.2 Preparation steps:
[0030] (1) Add 130kg deionized water into the reaction kettle, stir, add ammonium persulfate and sodium sulfite, stir for 0.5h, pump into the meterin...
Embodiment 2
[0034] 2.1 A fluid loss reducing agent for high temperature and compound salt polymers for drilling fluids, which consists of the following raw materials in percentage by weight: 12.0% acrylic acid, 7.0% sodium hydroxide, 62.0% deionized water, 7.0% acrylamide, four Sodium styrene sulfonate 5.3%, N-vinylpyrrolidone 6.5%, initiator 0.2%.
[0035] Prepare 1000 kg of fluid loss reducing agent for high temperature and anti-compound salt polymer for drilling fluid of the present invention, specific raw materials and consumption are: 120 kg of acrylic acid, 70 kg of sodium hydroxide, 620 kg of deionized water, 70 kg of acrylamide, tetraphenylethylene sulfonic acid Sodium 53kg, N-vinylpyrrolidone 65kg, initiator 2kg, wherein initiator is potassium persulfate 1kg, sodium bisulfite 1kg.
[0036] 2.2 Preparation steps:
[0037] (1) Add 186kg of deionized water into the reaction kettle, stir, add potassium persulfate and sodium bisulfite, stir for 0.5h, pump into the metering tank for u...
Embodiment 3
[0041] 3.1 A fluid loss reducing agent for high temperature and compound salt polymers for drilling fluids, which consists of the following raw materials in percentage by weight: 15.0% acrylic acid, 8.5% sodium hydroxide, 60.0% deionized water, 4.0% acrylamide, four Sodium styrene sulfonate 5.6%, N-vinylpyrrolidone 6.5%, initiator 0.4%.
[0042]Prepare 1000kg of water loss reducing agent for high temperature and anti-compound salt polymer for drilling fluid of the present invention, the specific raw materials and consumption are: 150kg of acrylic acid, 85kg of sodium hydroxide, 600kg of deionized water, 40kg of acrylamide, tetraphenylethylene sulfonic acid Sodium 56kg, N-vinylpyrrolidone 65kg, initiator 4kg, wherein initiator is ammonium persulfate 2kg, sodium bisulfite 2kg.
[0043] 3.2 Preparation steps:
[0044] (1) Add 150kg deionized water into the reaction kettle, stir, add potassium persulfate and sodium bisulfite, stir for 0.5h, pump into the metering tank for use;
...
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