Lithium-ion battery cathode material lithium iron phosphate and preparation method thereof
A technology for lithium ion batteries and positive electrode materials, applied in the field of lithium ion battery positive electrode materials and their preparation, can solve the problems of complex process operation steps, irreversible capacity loss, pollution caused by the environment, etc., so as to improve the cycle performance and speed up the kinetics of lithium storage. , the effect of high production efficiency
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Embodiment 1
[0038] a kind of like figure 1 Lithium-ion battery cathode material LiFePO shown in the present invention 4 , the lithium-ion battery cathode material LiFePO 4 the D 50 At 1.86μm, specific surface area at 19.25m 2 / g, tap density 1.54g / cm 3 .
[0039] Lithium-ion battery cathode material LiFePO of the present embodiment 4 It is prepared by using iron phosphate as a raw material with a nano-ceramic grinding and dispersing machine, and specifically includes the following steps:
[0040] (1) Raw material preparation: purchase iron phosphate (iron source and phosphorus source), lithium hydroxide and glucose as raw materials; according to LiFePO 4The molecular formula is used for batching; the dosage of glucose is calculated according to 6% of the theoretical carbon content; considering the burning loss of lithium source and phosphorus source in the sintering process, a small amount of surplus is required for lithium source and phosphorus source, so lithium source and iron so...
Embodiment 2
[0046] a kind of like figure 2 Lithium-ion battery cathode material LiFePO shown in the present invention 4 , the lithium-ion battery cathode material LiFePO 4 the D 50 At 5.3μm, specific surface area at 15.74m 2 / g, tap density 1.55g / cm 3 .
[0047] Lithium-ion battery cathode material LiFePO of the present embodiment 4 It is prepared by using iron phosphate as a raw material with a nano-ceramic grinding and dispersing machine, and specifically includes the following steps:
[0048] (1) Raw material preparation: purchase iron phosphate (iron source and phosphorus source), lithium hydroxide and glucose as raw materials; according to LiFePO 4 The molecular formula is used for batching; the dosage of glucose is calculated according to 6% of the theoretical carbon content; considering the burning loss of lithium source and phosphorus source in the sintering process, a small amount of surplus is required for lithium source and phosphorus source, so lithium source and iron s...
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