Lithium ion battery ternary cathode material modified by nanometer SnO2 and preparation method of lithium ion battery ternary cathode material
A technology for lithium-ion batteries and positive electrode materials, applied in the field of nano-SnO2 modified lithium-ion battery ternary positive electrode materials and its preparation, can solve problems such as undiscovered ternary positive electrode materials, avoid agglomeration growth, improve repeatability and consistency , the effect of high capacity
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[0030] LiNi produced by 3M Company 1 / 3 co 1 / 3 mn 1 / 3 o 2 As the modified body, it is used as the product design.
[0031] Preparation: mix HCl and deionized water by volume V HCl :V H2O =1:4 configured as an aqueous solution; 15wt% ammonia aqueous solution.
[0032] Preparation Process:
[0033] First, boil the purchased nano-carbon in 0.2 mol / L aqueous nitric acid solution for 30 minutes, filter and wash, then boil the washed nano-carbon in 0.1 mol / L sodium hydroxide aqueous solution for 30 minutes, then filter and wash, at 80°C drying. After drying in N 2 In atmosphere, activate at 500°C for 30min.
[0034] At 20°C, take 100ml of deionized water, adjust the pH to 2.2 with 1:4 hydrochloric acid, add 4.2072g of SnCl 4 ·6H 2 O was stirred and dissolved, and after the solution was clarified, 6ml of 15wt% aqueous ammonia solution was added dropwise, and after stirring for 2h, 6ml of 15wt% aqueous ammonia solution was added dropwise. Stirring was continued for 14 hours...
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