Multi-element composite flocculant for treating printing and dying wastewater and textile wastewater and preparing method thereof
A multi-component composite and flocculant technology, applied in the direction of flocculation/sedimentation water/sewage treatment, etc., can solve the problems of difficulty in universal application, high treatment cost, slow flocculation and sedimentation speed, etc., and achieve broad industrialization prospects and market value, COD High removal rate and wide pH application range
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preparation example 1
[0034] Preparation Example 1: Preparation of Polyaluminum Calcium Chloride
[0035] Weigh 150 g of alumina and 150 g of calcium carbonate and mix them uniformly, heat and react at 850 °C for 8 h, then cool to room temperature at a cooling rate of 8 °C / min to obtain an intermediate product, which is dissolved in 450 g React in hydrochloric acid with a mass concentration of 50-60% for 2 h, evaporate to dryness to obtain solid polyaluminum calcium chloride, and set aside.
preparation example 2
[0036] Preparation Example 2: Preparation of Aluminum Magnesium Titanium Polysilicate
[0037] Prepare a sodium silicate aqueous solution with a mass concentration of 4%, add sulfuric acid with a mass concentration of 40% to adjust pH=4, stir and react at room temperature for 30 min, then add aluminum chloride, magnesium sulfate and titanium chloride to the solution to make the aluminum salt The molar ratio of metal ions to silicon in , magnesium salt and titanium salt is 0.6:1. After stirring evenly, the temperature is raised to 70°C at a heating rate of 4°C / min, aged at this temperature for 2 days, and titanium is obtained after drying and solidification. Magnesium aluminum polysilicate.
preparation example 3
[0038] Preparation Example 3: Preparation of Aluminum Hydroxide Gel
[0039] Weigh 50 g of crystalline aluminum hydroxide, add 300 g of hydrochloric acid with a mass concentration of 50% by weight and 400 g of water, dissolve it at 105°C and 0.2 Mpa, react for 8 hours, cool and precipitate to obtain Aluminum hydroxide gel.
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