Formula and preparation method of high-molecular LED (Light Emitting Diode) radiation material
A heat-dissipating material and polymer technology, which is applied to the formulation of polymer LED heat-dissipating materials and the field of preparation thereof, can solve the problems of hindering heat dissipation of high-power LED lamps, complicated molding process, and high cost, and achieves light weight, simple molding process, and high cost. low cost effect
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Embodiment 1
[0027] The filler includes graphite powder and acetylene carbon black at a ratio of 1:1, dried at 120°C for 30 minutes and cooled to 25°C for use;
[0028] Component A includes: 665 organosilicon epoxy resin 80kg, FB high temperature resistant flame retardant thermosetting phenolic resin 20kg, filler 20kg, mix 665 organosilicon epoxy resin and FB high temperature resistant flame retardant thermosetting phenolic resin at 25℃~30℃ After uniformity, add the filler slowly and stir well until it is evenly mixed and set aside;
[0029] Component B includes: 200# low molecular weight polyamide 20kg, polyethylene polyamine (PEPA) 12kg, N-303 trihydroxy polyether polyol 37kg, DMP-302, 4,6-tris(dimethylaminomethyl)phenol 3kg, KH-550 coupling agent 0.5kg, zinc powder 1kg, antioxidant 1010 0.1kg, ultraviolet absorber UV-327 0.1kg, filler 46kg, put the components except filler at 25℃~30℃ After stirring evenly, add the filler slowly and stir well until it is evenly mixed and set aside;
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Embodiment 2
[0032] The filler includes graphite powder, polyphenylene powder and acetylene carbon black at a ratio of 1:1:1, dried at 110°C for 40 minutes and cooled to 25°C for use;
[0033] Component A includes 85kg of 665 organosilicon epoxy resin, 25kg of FB high temperature resistant flame retardant thermosetting phenolic resin, 25kg of filler, stir 665 organosilicon epoxy resin and FB high temperature resistant flame retardant thermosetting phenolic resin at 25℃~30℃ Then add the filling slowly and stir well until it is evenly mixed and ready for use;
[0034] Component B includes 200# low molecular weight polyamide 25kg, polyethylene polyamine (PEPA) 14kg, N-303 trihydroxy polyether polyol 40kg, DMP-302, 4,6-tris(dimethylaminomethyl)phenol 4kg , KH-550 coupling agent 0.6kg, zinc powder 1.1kg, antioxidant 1010 0.09kg, ultraviolet absorber UV-327 0.12kg, filler 48kg, put the components except filler at 25℃~30℃ After stirring evenly, add the filler slowly and stir well until it is eve...
Embodiment 3
[0037] The filler includes ultra-fine ferrophosphorus powder and acetylene carbon black at a ratio of 1:1, dried at 115°C for 40 minutes and cooled to 25°C for use;
[0038] Component A includes 75kg of 665 organosilicon epoxy resin, 15kg of FB high temperature resistant flame retardant thermosetting phenolic resin, 15kg of filler, stir 665 organosilicon epoxy resin and FB high temperature resistant flame retardant thermosetting phenolic resin at 25℃~30℃ Then add the filling slowly and stir well until it is evenly mixed and ready for use;
[0039] Component B includes 15kg of 200# low-molecular polyamide, 10kg of polyethylene polyamine (PEPA), 35kg of N-303 trihydroxy polyether polyol, DMP-302, 2kg of 4,6-tris(dimethylaminomethyl)phenol , KH-550 coupling agent 0.4kg, zinc powder 0.9kg, antioxidant 1010 0.12kg, ultraviolet absorber UV-327 0.08kg, filler 44kg, put the components except filler at 25℃~30℃ After stirring evenly, add the filler slowly and stir well until it is even...
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