Method for preparing beryllium-copper alloy sheet by adopting continuous multi-arc ion plating physical vapour deposition

A technology of physical vapor deposition and multi-arc ion plating, applied in ion implantation plating, sputtering plating, vacuum evaporation plating, etc., can solve the technical difficulties of low production efficiency, beryllium metal polluting the environment, and rolling beryllium copper alloy Large and other problems, to achieve the effect of low manufacturing cost, high product yield, simple and easy process

Active Publication Date: 2013-04-03
兰州大成科技股份有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen that the technical difficulty of rolling beryllium copper alloy is high, and the yield and production efficiency are low.
Moreover, beryllium copper alloys are smelted in an atmospheric environment, and there are disadvantages such as beryllium metal polluting the environment.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Embodiment 1: a kind of method that adopts continuous multi-arc ion plating physical vapor deposition method to prepare beryllium-copper alloy thin plate, its steps are:

[0026] Step 1. Select a pure copper strip with a thickness of 0.1-0.25mm as the substrate, and do the following pretreatment:

[0027] (1) Wash with sodium carbonate lye at a concentration of 3-5% and a temperature of 60-80°C for 3-5 minutes to remove oil stains;

[0028] (2) Wash with dilute sulfuric acid at a concentration of 3 to 5% for 3 to 5 minutes to remove scale;

[0029] (3) Rinse with clean water;

[0030] (4) Ultrasonic cleaning with anhydrous ethanol, drying for later use;

[0031] Step 2. Select pure Be target or high beryllium content beryllium copper (50 ~ 80wt.%Be) alloy target:

[0032] preparation Pure Be or beryllium copper with high Be content (50-80wt.%Be) alloy target is used as a multi-arc ion plating target and is ready for use;

[0033] Step 3. Install the pure copper s...

Embodiment 2

[0046] Example 2 Multi-arc ion plating vapor deposition single-sided Be infiltrated

[0047] Step 1: Select pure copper substrate

[0048] Select a 200mm × 200mm, 0.20mm thick pure copper strip as the substrate, first wash it with a sodium carbonate solution with a concentration of 5% and a temperature of 60°C for 5 minutes to remove oil stains; then wash it with a concentration of 4% dilute hydrochloric acid for 3 minutes to remove oxidation skin; then rinse with clean water; then ultrasonically clean with anhydrous ethanol, and dry for later use.

[0049] Step 2: Select pure Be target

[0050] select Pure Be target material, ready for use;

[0051] Step 3: Install the pure copper strip treated in step 1 on the substrate of a multi-arc ion coating machine as an anode; then put the pure Be target processed in step 2 into a multi-arc ion coating machine as a cathode;

[0052] Vacuum to 2×10 -3 After Pa, pass argon to stabilize the pressure in the multi-arc ion coating machi...

Embodiment 3

[0059] Example 3 Multi-arc ion plating vapor deposition single-sided Be infiltration

[0060] Step 1: Select pure copper substrate

[0061] Select a 200mm×200mm, 0.15mm thick pure copper strip as the substrate, first wash it with a sodium carbonate solution with a concentration of 5% and a temperature of 60°C for 5 minutes to remove oil stains; then wash it with dilute hydrochloric acid with a concentration of 4% for 3 minutes to remove oxidation skin; then rinse with clean water; then ultrasonically clean with anhydrous ethanol, and dry for later use.

[0062] Step 2: Select a beryllium copper alloy target with high Be content

[0063] casting Beryllium copper (Cu-80wt.%Be) alloy target with high Be content, ready for use;

[0064] Step 3: Install the pure copper strip treated in step 1 on the substrate of the multi-arc ion coating machine as the anode; then put the beryllium copper alloy target treated in step 2 into the multi-arc ion coating machine as the cathode ;

...

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Abstract

The invention relates to a method for preparing a beryllium-copper alloy sheet, in particular to a method for preparing a high-quality beryllium-copper alloy sheet by adopting continuous multi-arc ion plating physical vapour deposition. The method for preparing the beryllium-copper alloy sheet by adopting the continuous multi-arc ion plating physical vapour deposition comprises the following steps: by using a pure Be metal target or a beryllium-copper alloy target with high beryllium content as a cathode, using a pure copper strip as an anode and adopting the multi-arc ion plating physical vapour deposition, depositing a pure Be or Be-rich film which is well combined on the single surface or on double surfaces of the pure copper strip; and then carrying out high temperature diffusion treatment to enable Be atoms to be diffused to permeate a pure copper matrix until the Be content in the copper strip reaches 1 to 3 weight percent, so that a Be alloy strip with excellent mechanical performance and electrical conductivity and Cu content of minus 1 to 3 weight percent is obtained. The method disclosed by the invention is simple and easy to operate, has high working efficiency, is energy-saving and environmental-friendly in the preparing process, has controllable quality and is very suitable for industrial application.

Description

technical field [0001] The present invention relates to a method for preparing a beryllium-copper alloy sheet, more particularly, a method for preparing a high-performance beryllium-copper alloy sheet by using continuous multi-arc ion plating physical vapor deposition. Background technique [0002] Beryllium-copper alloy is a typical precipitation-strengthened alloy, which has a series of advantages such as high elasticity, high strength, high conductivity, corrosion resistance, fatigue resistance, small elastic hysteresis, non-magnetism, and no sparks during impact. It is widely used It is used in aerospace, aviation, electronics, communication, machinery, petroleum, chemical industry, automobile and home appliance industries, and has broad application prospects. [0003] At present, beryllium-copper alloy sheets and strips are basically prepared by rolling method, mainly including semi-continuous casting ingot + milling skin + heating + rough rolling + quenching + secondar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C14/32C23C14/16
Inventor 范多进田广科范多旺陈虎孔令刚马海林孙勇
Owner 兰州大成科技股份有限公司
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