Lead-free aluminum solder wire and preparation method thereof
A tin wire and aluminum welding technology, applied in welding equipment, welding medium, manufacturing tools, etc., can solve the problems of flux leakage, poor solderability, product scrapping, etc., to reduce the scrap rate, reduce the difficulty of cleaning, The effect of saving tin solder
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[0032] The preparation method of hydroxylamine fluoride comprises the following steps:
[0033] 1) In terms of weight percentage, take 1-5% of ethylenediamine, 3-30% of ethanolamine, 20-90% of diethanolamine and 5-80% of triethanolamine, and mix them uniformly to obtain a mixture;
[0034] 2) Neutralize the resulting mixture with hydrofluoric acid to a pH value of 6.5-8;
[0035] 3) Evaporate the above neutralized product at a temperature of 140-160°C for 3.5-4.5 hours.
[0036] The metal active salt is one or more of tin fluoride, stannous fluoride, stannous fluoroborate, stannous chloride, zinc fluoride, zinc fluoroborate, zinc chloride and bismuth chloride combination.
[0037] The activator is one or a combination of diethylamine hydrochloride, triethylamine hydrochloride, lithium fluoride, sodium fluoride, magnesium fluoride and aluminum fluoride.
[0038] The corrosion inhibitor is benzotriazole and / or piperazine.
[0039] A method for preparing lead-free aluminum so...
Embodiment 1
[0049]The preparation method of hydroxylamine fluoride, it may further comprise the steps:
[0050] 1) According to weight percentage, take ethylenediamine 1%, ethanolamine 30%, diethanolamine 64% and triethanolamine 5%, mix and stir evenly to obtain a mixture;
[0051] 2) neutralize the resulting mixture with hydrofluoric acid to a pH value of 6.5;
[0052] 3) Evaporate the above-mentioned neutralized product at 140°C for 4.5 hours to remove the moisture and prevent subsequent welding spatter.
Embodiment 2
[0054] The preparation method of hydroxylamine fluoride, it may further comprise the steps:
[0055] 1) According to weight percentage, take 5% ethylenediamine, 3% ethanolamine, 84% diethanolamine and 8% triethanolamine, mix and stir evenly to obtain a mixture;
[0056] 2) Neutralize the resulting mixture to a pH of 8 with hydrofluoric acid;
[0057] 3) Evaporate the above-mentioned neutralized product at 160°C for 3.5 hours to remove the moisture and prevent subsequent welding spatter.
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