Preparation method of catalyst for producing 1,2-cyclohexane dicarboxylic ester through hydrogenation
A cyclohexanedicarboxylate and catalyst technology, applied in the field of catalysis, can solve the problems of complex catalyst preparation process, high reaction temperature, unfavorable reaction progress and the like
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Embodiment 1
[0027] Take 100g of activated alumina spherical carrier (specific surface 190.34m 2 / g, pore diameter 10.5nm, pore volume 0.51ml / g, ball diameter 5mm), and dried at 110℃ for 12h for later use. RuCl containing 0.1g Ru elemental 3 Impregnate 100 g of the carrier with an equal volume of hydrochloric acid aqueous solution for 3 hours, dry at 110°C for 10 hours after impregnation, and heat up to 300°C for 3 hours. Soak the catalyst with 0.5wt% NaOH aqueous solution, slightly heat, boil and wash 3 times. The catalyst was washed with deionized water, dried in the air, and dried at 120° C. for 10 h. Prepare Ru / Al with 0.1% Ru elemental mass fraction 2 o 3 catalyst.
Embodiment 2
[0029] Take 100g of activated alumina spherical carrier (specific surface 190.34m 2 / g, pore diameter 10.5nm, pore volume 0.51ml / g, ball diameter 5mm), and dried at 110℃ for 12h for later use. RuCl containing 0.5g Ru elemental 3 Impregnate 100 g of the carrier with an equal volume of hydrochloric acid aqueous solution for 5 hours, dry at 110°C for 10 hours after impregnation, and heat up to 300°C for 3 hours. Soak the catalyst with 0.5wt% NaOH aqueous solution, heat slightly, boil and wash 6 times. The catalyst was washed with deionized water, dried in the air, and dried at 120° C. for 10 h. Prepare Ru / Al with 0.5% Ru mass fraction 2 o 3 catalyst.
Embodiment 3
[0031] Take 100g of activated alumina spherical carrier (specific surface 190.34m 2 / g, pore diameter 10.5nm, pore volume 0.51ml / g, ball diameter 5mm), and dried at 110℃ for 12h for later use. Ru(NO 3 ) 3 Impregnate 100 g of the carrier with an equal volume of hydrochloric acid aqueous solution for 8 hours, dry at 110°C for 10 hours after impregnation, and heat up to 300°C for 3 hours. Soak the catalyst with 2.0wt% NaOH aqueous solution, heat slightly, boil and wash 3 times. The catalyst was washed with deionized water, dried in the air, and dried at 120° C. for 10 h. Prepare Ru / Al with 2.0% Ru mass fraction 2 o 3 catalyst.
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