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A kind of SIC reinforced aluminum matrix composite material and preparation method thereof for spacecraft

A composite material and reinforced aluminum-based technology, which is applied in the field of SiC reinforced aluminum-based composite materials and its preparation for spacecraft, can solve the problems of affecting the stability of material strength, large differences in thermal expansion coefficients, and easy thermal cycle stress, etc., to achieve Reduce the generation of voids, reduce the coefficient of thermal expansion, and enhance the effect of uniform distribution of phases

Active Publication Date: 2014-10-29
HENAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Cu / Mo alloy and Cu / W alloy have high thermal conductivity and matching thermal expansion coefficient, but the price of Mo and W is high, the processing and welding performance is poor, and the density is high, so it is not suitable for application in the aerospace field
[0004] As a hotspot in the research of composite materials, there are many research results on SiC reinforced aluminum matrix composite materials published in the world at home and abroad. However, due to the large difference in thermal expansion coefficient between SiC and aluminum or its alloys, large residual stress remains in the structure. The follow-up processing is complicated, and it is easy to cause thermal cycle stress in the working environment, which affects the stability of material strength

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] The composition and weight percentage of a SiC-reinforced aluminum-based composite material for spacecraft in this embodiment are: SiC 26%, Si 33%, Mg 2%, and the balance is Al and unavoidable impurities.

[0018] The specific preparation method of the present embodiment is as follows:

[0019] (1) First soak the SiC powder with HF with a volume fraction of 10% for 2 hours, then wash it with distilled water, vacuum filter, and dry it; then roast the SiC powder at 1100°C for 3 hours; Carry out anhydrous ethanol ultrasonic vibration cleaning for 10 minutes, then wash with distilled water, vacuum filter, and dry;

[0020] (2) Mix SiC powder, Al-30Si powder, and Mg powder by vacuum wet high-energy ball milling, use absolute ethanol as the medium, time is 4 hours, and the rotation speed is 230r / min. After the mixing is completed, put the slurry Dry in a vacuum oven;

[0021] (3) Apply absolute ethanol with a mass fraction of 40% and corundum powder with a mass fraction of ...

Embodiment 2

[0024] The composition and weight percentage of a SiC-reinforced aluminum-based composite material for spacecraft in this embodiment are: SiC 27%, Si 29%, Mg 1.9%, and the balance is Al and unavoidable impurities.

[0025] The specific preparation method of the present embodiment is as follows:

[0026] (1) First soak the SiC powder with HF with a volume fraction of 10% for 2 hours, then wash it with distilled water, vacuum filter, and dry it; then roast the SiC powder at 1100°C for 3 hours; Carry out anhydrous ethanol ultrasonic vibration cleaning for 10 minutes, then wash with distilled water, vacuum filter, and dry;

[0027] (2) Mix SiC powder, Al-30Si powder, and Mg powder by vacuum wet high-energy ball milling, use absolute ethanol as the medium, time is 3 hours, and the rotation speed is 250r / min. After the mixing is completed, put the slurry Dry in a vacuum oven;

[0028] (3) Smear absolute ethanol with a mass fraction of 40% and corundum powder with a mass fraction o...

Embodiment 3

[0031] The composition and weight percentage of a SiC-reinforced aluminum-based composite material for spacecraft in this embodiment are: SiC 30%, Si 28%, Mg 1.8%, and the balance is Al and unavoidable impurities.

[0032] The specific preparation method of the present embodiment is as follows:

[0033](1) First soak the SiC powder with HF with a volume fraction of 10% for 2 hours, then wash it with distilled water, vacuum filter, and dry it; then roast the SiC powder at 1100°C for 3 hours; Carry out anhydrous ethanol ultrasonic vibration cleaning for 10 minutes, then wash with distilled water, vacuum filter, and dry;

[0034] (2) Mix SiC powder, Al-30Si powder, and Mg powder by vacuum wet high-energy ball milling, using absolute ethanol as the medium, for 5 hours, and the rotation speed is 240r / min. After the mixing is completed, place the slurry Dry in a vacuum oven;

[0035] (3) Smear absolute ethanol with a mass fraction of 40% and corundum powder with a mass fraction of...

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Abstract

The invention discloses a SiC enhanced aluminum-based composite material for a spacecraft and a preparation method thereof. The composite material consists of the following chemical ingredients in percentage by weight: 23 to 35 percent of SiC, 26 to 35 percent of Si, 1.8 to 2.0 percent of Mg and the balance of Al and inevitable impurities. The method comprises the following steps of: performing surface treatment of powder, performing high-energy ball-milling mixing under vacuum by a wet method, and performing hot pressed sintering under the vacuum. The thermal expansivity and density of the material can be reduced effectively and the tensile strength can be improved by controlling the addition of the SiC and an alloy element Mg and a preparation process, so that the composite material which is low in cost and high in corrosion resistance and of which the thermal expansivity is 7 to 9*10<-6> / DEG C, the density is less than 2.7 g / cm<3> and the tensile strength is more than 230 MPa is obtained. The SiC enhanced aluminum-based composite material is particularly suitable for aerospace parts which are light in mass, low in expansion and resistant to corrosion and have certain strength.

Description

technical field [0001] The invention belongs to the field of metal matrix composite material manufacturing, and in particular relates to a SiC reinforced aluminum matrix composite material used for spacecraft and a preparation method thereof. Background technique [0002] In the design of spacecraft, dimensional stability is widely used in high-precision instruments, inertial platforms and other fields. Due to the large range of temperature changes in the working environment and the needs of the instrument itself, especially some optoelectronic equipment, it is required that the materials used should be stable when the temperature changes. The dimensional change is very small, which requires the thermal expansion coefficient of the material to be very small, or even zero; the material needs to have stable tensile strength, and the cyclic thermal stress is required to be very small. In order to increase the payload of the spacecraft, it is necessary to further reduce the dens...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C32/00C22C21/00C22C1/05
Inventor 王爱琴倪增磊谢敬佩李继文李洛利王文焱孙浩亮郝世明
Owner HENAN UNIV OF SCI & TECH
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