Ultrasonic-assisted supercritical CO2 (carbon dioxide) wool fiber dyeing process
An ultrasonic and supercritical technology, applied in the field of dyeing process, can solve the problems of damage and heat preservation, high process requirements, failure to meet export standards, etc., and achieve the effect of small damage, short dyeing time and simple process steps
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Embodiment 1
[0017] An ultrasonic-assisted supercritical CO 2 Wool fiber dyeing process, comprises the steps:
[0018] Step 1. Pretreatment: select, wash and classify the raw animal wool;
[0019] Step 2. Put the pretreated animal hair into an ultrasonic cell pulverizer with 3% cellulase of wool mass for ultrasonic treatment. The treatment temperature is 20°C, the ultrasonic power is 150W, and the treatment time is 10 minutes;
[0020] Step three, carry out supercritical CO to the animal hair after step two treatment 2 dyeing. When dyeing, add 2% cellulase of wool mass. Among them, CO 2 The flow rate is 5kg / h, the temperature is 30°C, the pressure is 30MPa, the liquor ratio is 20:1, the pH is controlled at 4-6, and the dyeing time is 15min.
Embodiment 2
[0022] An ultrasonic-assisted supercritical CO 2 Wool fiber dyeing process, comprises the steps:
[0023] Step 1. Pretreatment: select, wash and classify the raw animal wool;
[0024] Step 2. Put the pretreated animal hair into an ultrasonic cell pulverizer added with 10% cellulase of wool mass for ultrasonic treatment. The treatment temperature is 25° C., the ultrasonic power is 200 W, and the treatment time is 7 minutes. ;
[0025] Step three, carry out supercritical CO to the animal hair after step two treatment 2 dyeing. When dyeing, add 2% cellulase of wool mass. Among them, CO 2 The flow rate is 7kg / h, the temperature is 40°C, the pressure is 28MPa, the pH is controlled at 4.5-5, and the dyeing time is 10min.
Embodiment 3
[0027] An ultrasonic-assisted supercritical CO 2 Wool fiber dyeing process, comprises the steps:
[0028] Step 1. Pretreatment: select, wash and classify the raw animal wool;
[0029] Step 2. Put the pretreated animal hair into an ultrasonic cell pulverizer added with 3% cellulase of wool mass for ultrasonic treatment. The treatment temperature is 40° C., the ultrasonic power is 300 W, and the treatment time is 7 minutes. ;
[0030] Step three, carry out supercritical CO to the animal hair after step two treatment 2 dyeing. When dyeing, add 2% cellulase of wool mass. Among them, CO 2 The flow rate is 5kg / h, the temperature is 35°C, the pressure is 25MPa, the pH is controlled at 4.5-5, and the dyeing time is 10min.
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