Lithium silicate ceramic material absorbing high-temperature carbon dioxide and preparation method thereof
A technology of carbon dioxide and ceramic materials, which is applied in the field of preparation of lithium silicate ceramic materials, can solve the problems of high sintering temperature and low carbon dioxide adsorption rate, and achieve the effects of low sintering temperature, easy industrial production, and simple process
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Embodiment 1
[0013] Use an electronic balance to weigh SiO 2 20.25g, Li 2 CO 3 48.75g, K 2 CO 3 It is 0.917g, put it into a mortar, grind it to make it powdery and reach the micron level, and then put it into a high-temperature resistance furnace for sintering at 750 ° C, and keep it warm for 2 hours and 6 hours respectively to obtain a silicic acid that absorbs high-temperature carbon dioxide lithium ceramic material.
[0014] Fully grind the prepared K-doped lithium silicate ceramic material, put it into a thermogravimetric analyzer in the range of room temperature to 900°C, and keep the temperature at 750°C for 20 minutes to test its adsorption capacity for carbon dioxide. At equilibrium, the adsorption rates are 14.31wt% and 22.62wt%, respectively.
Embodiment 2
[0016] Referring to Example 1, the sample was weighed and ground, and sintered in a high-temperature furnace at 850°C, kept for 2 hours and 6 hours respectively, and then the obtained sample was also ground and tested under the same conditions. When the absorption equilibrium was reached, the adsorption The ratios are 20.73wt% and 27.88wt% respectively.
Embodiment 3
[0018] Referring to Example 1, the sample was weighed and ground, and sintered in a high-temperature furnace at 900°C, kept for 2 hours and 6 hours respectively, and then the obtained sample was also ground and tested under the same conditions. When the absorption equilibrium was reached, the adsorption The ratios are 36.28wt% and 49.69wt% respectively.
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Abstract
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