Modified acrylate heat-dissipation powder coating as well as preparation method and application thereof
A powder coating and acrylate technology, applied in the field of its preparation and modified acrylate heat dissipation powder coating, can solve the problems of unfavorable heat conduction and heat dissipation, affecting the heat dissipation effect, and excessive particle diameter, so as to increase the effective heat dissipation area and facilitate the heat dissipation. The effect of conduction and improving heat dissipation efficiency
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Embodiment 1
[0062] 0.2g azobisisobutyronitrile and 30g xylene are formulated into initiator solution, and 1.5g carboxyl content is the multi-walled carbon nanotube (diameter 40nm, length 400nm) of 0.4% and 8.5g carbon fiber (carboxyl content is 0.02%) Carboxylated pitch-based carbon fiber, diameter 7000nm, length 5000nm), 10g styrene, 35g methyl methacrylate, 30g glycidyl methacrylate, 15g 2-ethylhexyl acrylate, 300g xylene formulated as a monomer solution;
[0063] In the reactor with material mixing function and temperature control function, the temperature of the monomer solution is raised to 65 ° C, and the initiator solution is added dropwise to the monomer solution for polymerization reaction in 4 times, and the time of each drop is 15 minutes. After the addition, the reaction was continued for 1 hour. When all the initiator solution was added to the polymerization system, the reaction was continued for 1 hour, and the synthesis reaction was completed to obtain a coating solution. ...
Embodiment 2
[0070] 0.2g azobisisobutyronitrile and 50g toluene are mixed with initiator solution, and 1.5g carboxyl content is the multi-walled carbon nanotube (diameter 40nm, length 400nm), 1g nano-alumina (diameter 300nm), 1.5 g nano silicon carbide (diameter 300nm) and 16g carbon fiber (carboxyl content is 0.02% carboxylated pitch-based carbon fiber, diameter 7000nm, length 5000nm), 8g styrene, 32g methyl methacrylate, 26g glycidyl methacrylate, 14g acrylate-2-ethylhexyl ester, 250g toluene is mixed with monomer solution;
[0071] In the reactor with material mixing function and temperature control function, the temperature of the monomer solution was raised to 72°C, and the initiator solution was added dropwise to the monomer solution in 4 times to carry out the polymerization reaction. The time for each drop was 15 minutes. After the addition, the reaction was continued for 1 hour. When all the initiator solution was added to the polymerization system, the reaction was continued for ...
Embodiment 3
[0076] 0.3g azobisisoheptanonitrile and 40g dimethylbenzene are formulated into initiator solution, and 1g hexagonal boron nitride (diameter 400nm), 1g nano-silicon carbide (diameter 200nm), 0.5g carboxyl content are 0.4% multi-walled carbon Nanotubes (diameter 40nm, length 400nm), and 12.5g carbon fiber (carboxyl group content is 0.04% carboxylated pitch-based carbon fiber, diameter 7000nm, length 5000nm), 10g styrene, 30g methyl methacrylate, 30g methacrylic acid shrink Glycerides, 15g of 2-ethylhexyl acrylate, and 300g of xylene are prepared into a monomer solution;
[0077] In the reactor with material mixing function and temperature control function, the temperature of the monomer solution was raised to 72°C, and the initiator solution was added dropwise to the monomer solution in 4 times to carry out the polymerization reaction. The time for each drop was 15 minutes. After the addition, the reaction was continued for 1 hour. When all the initiator solution was added to t...
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