Double-coated hollow glass microbead heat-insulated coating and preparation method thereof
A technology of hollow glass microspheres and thermal insulation coatings, applied in the direction of reflection/signal coatings, coatings, etc., can solve the problems that hollow glass microspheres are not easy to disperse, difficult to achieve reflection effect, affect the uniformity of coating film, etc., and achieve heat insulation The effect is obvious, the reflectivity and weather resistance are improved, and the product performance is stable
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Embodiment 1
[0024] (a) Preparation of titanium dioxide-coated hollow glass microspheres: Take 1 part of hollow glass microspheres according to the formula ratio, 10 parts of water, 0.21 parts of surfactant (sodium dodecylbenzenesulfonate solution), and 23 parts of titanium sulfate solution , 30 parts of sodium hydroxide solution, put hollow glass microspheres in a four-neck flask, add water to make a slurry; put the slurry in a constant temperature water bath at 55°C, and stir thoroughly for 10-15min; add a surfactant, Add sodium hydroxide solution dropwise to control the system pH=6~8; slowly add titanium sulfate solution dropwise, and the reaction lasts for 6 hours; after the reaction is completed, wash with water, filter, dry, and finally calcined at 600°C to obtain titanium dioxide-coated hollow glass beads Product; (b) Preparation of hollow glass microspheres coated with iron oxide: take 1 part of hollow glass microspheres prepared above according to the formula ratio, 10 parts of wat...
Embodiment 2
[0026](a) Preparation of titanium dioxide-coated hollow glass microspheres: take 1.4 parts of hollow glass microspheres according to the formula ratio, 11 parts of water, 0.24 parts of surfactant (sodium dodecylbenzenesulfonate solution), and 30 parts of titanium sulfate solution , 37 parts of sodium hydroxide solution, put hollow glass microspheres in a four-neck flask, add water to make a slurry; put the slurry in a constant temperature water bath at 55°C, and stir fully for 10-15min; add a surfactant, Add sodium hydroxide solution dropwise to control the system pH=6~8; slowly add titanium sulfate solution dropwise, and the reaction lasts for 6 hours; after the reaction is completed, wash with water, filter, dry, and finally calcined at 600°C to obtain titanium dioxide-coated hollow glass beads Product; (b) Preparation of iron oxide re-coated hollow glass microspheres: take 1.4 parts of hollow glass microspheres prepared above according to the formula ratio, 10 parts of water...
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