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Method for preparing Ni-Zn ferrite film

A ferrite thin film, ni-zn technology, applied in the direction of ion implantation plating, coating, metal material coating process, etc., can solve the problem that there is no obvious effect on the improvement of microwave magnetic properties of ferrite thin film, and no iron is seen. Oxygen thin film soft magnetic properties and microwave magnetic properties, weakening and other issues, to achieve the effect of improving soft magnetic and microwave properties, optimizing soft magnetic properties, and improving soft magnetic properties

Inactive Publication Date: 2012-01-18
LANZHOU UNIVERSITY
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  • Application Information

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Problems solved by technology

Example: using ZnFe 2 o 4 As a substrate layer to improve the soft magnetic properties of Ni-Zn ferrite thin films: J.H.Gao, Y.T.Cui, and Z.Yang, "The magnetic properties of Ni x Zn 1-x Fe 2 o 4 films fabricated by alternative sputtering technology", Materials Science and Engineering B 110, 111-114 (2004); using YSZ (Y 0.15 Zr 0.85 o 2 ) as a substrate layer to prepare and improve the soft magnetic properties of Ni-Zn ferrite thin films: S.Y.Bae, C.S.Kim, and Y.J.Oh, "Magnetic properties of sol-gel derived Ni-Zn ferrite thin films on yttria stabilized zirconia buffered Si( 100)", Journal of Applied Physics 85, 5226-5228 (1999). This traditional method of using non-magnetic oxide as the substrate layer is to improve the softness of the ferrite film by weakening the stress between the substrate and the ferrite film. However, this traditional method only achieves the optimization of the soft magnetic properties of ferrite films (for example: saturation magnetization M s has been improved, the coercive force H c has been reduced), but there is no obvious effect on the improvement of the microwave magnetic properties of ferrite thin films
At the same time, in the existing reported literature, there is no method to effectively improve the soft magnetic properties and microwave magnetic properties of ferrite thin films at the same time.

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  • Method for preparing Ni-Zn ferrite film
  • Method for preparing Ni-Zn ferrite film
  • Method for preparing Ni-Zn ferrite film

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Embodiment Construction

[0016] The following Ni of the present invention is combined with the embodiment 0.45 Zn 0.55 Fe 2 O 4 The preparation of the film, its soft magnetic properties and the improvement of microwave magnetic properties will be explained. In the preparation process of this example, the equipment used to deposit the film is the FJI560-I ultra-high vacuum magnetron and The RF sputtering section of an ion beam sputtering apparatus. The sputtering equipment requires two RF magnetron targets: commercial high-purity (99.99%) Fe 50 Mn 50 The target material of the Ni-Zn ferrite film is prepared by the traditional co-precipitation method, and the Ni-Zn ferrite powder is prepared by pressing and sintering. The film deposition process is: first pump the vacuum of the vacuum chamber to 5.0×10 -5 Below, a layer of Fe with a thickness of 25nm is deposited on the single crystal Si(111) substrate under the condition that the RF power supply is 50W, the sputtering gas is high-purity Ar gas, a...

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Abstract

The invention discloses a method for preparing a ferrite film, in particular to a method which can obtain a spinel type Ni-Zn ferrite film with better soft magnetic and microwave properties. The method includes the following steps: first depositing a layer of antiferromagnetic material Fe50Mn50 on a substrate, and then depositing a Ni-Zn ferrite film layer on the Fe50Mn50 layer. The method can also prepare multiple layers of Ni-Zn ferrite films. The adoption of the method can enhance the soft magnetic and microwave properties of the prepared Ni-Zn ferrite film.

Description

technical field [0001] The invention relates to a method for preparing a Ni-Zn ferrite film, in particular to a method for obtaining a spinel type Ni-Zn ferrite film with better soft magnetic and microwave properties. Background technique [0002] In recent years, with the rapid development of communications, computers and high-density magnetic recording materials, the performance requirements for magnetic materials are getting higher and higher. Especially with the continuous improvement of information processing frequency (for example: mobile phones, wireless LAN systems and Bluetooth devices and other commonly used operating frequencies have increased to 1-5GHz), involving information storage and conversion (for example: inductors, transformers and electromagnetic shielding systems, etc. ) micromagnetic devices urgently require high-performance magnetic materials operating in the GHz range. Spinel-type Ni-Zn ferrite materials are widely used in transformers, high-frequen...

Claims

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Application Information

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IPC IPC(8): C23C14/06C23C14/14
Inventor 薛德胜郭党委蒋长军
Owner LANZHOU UNIVERSITY
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