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Preparation method of compound leather bactericidal and mildew-proof agent

A technology of bactericidal and mildew-proofing agent and leather, applied in the direction of fungicides, biocides, biocides, etc., can solve the problem that leather bactericidal and mildew-proofing treatment is not ideal.

Inactive Publication Date: 2012-01-18
覃终
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The object of the present invention is to provide a leather composite antibacterial and antifungal agent for the various disadvantages of the existing fungicide and antifungal agent and to solve the technical problems in the known technology. Preparation of fungicides, especially with guanidine compounds, 2-bromo-2-nitro-1,3-propanediol, butyl iodopropynylcarbamate, Torrolone B, corrosion inhibitors, ethanol and water The composition is prepared as a compound bactericide and antifungal agent for leather, which has the characteristics of safety, high efficiency, broad spectrum, low toxicity, and environmental protection.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] components kilogram kg Mass percentage % Polyhexamethyleneguanidine 10 10 Torrey B 0.3 0.3 2-Bromo-2-nitro-1,3-propanediol 1 1 95% ethanol 10 10 Butyl iodopropynylcarbamate 0.6 0.6 sodium benzoate 1.5 1.5 sodium salicylate 1.5 1.5 water 75.1 75.1 total 100 100

[0044] 1. Mix and stir polyhexamethyleneguanidine, 2-bromo-2-nitro-1,3-propanediol and Tuoliron B with 50% of the above mass percent water for 3 hours to prepare a mixed substance A;

[0045] 2. Mix butyl iodopropynyl carbamate, sodium benzoate, sodium salicylate, and ethanol with the remaining 50% of the above mass percentage and stir for 3 hours to prepare mixed substance B;

[0046] 3. Stir and react the above mixed substance A with the above mixed substance B for 2 hours, then let it stand for 2 hours, and mix the mixed substance

[0047] The content of the mixture is determined, and the qualified mixture is packaged as a qualif...

Embodiment 2

[0049] components kilogram kg Mass percentage % polyhexamethylene biguanide 8 8 Torrey B 0.3 0.3 2-Bromo-2-nitro-1,3-propanediol 1 1 95% ethanol 10 10 Butyl iodopropynylcarbamate 0.6 0.6 sodium benzoate 1 1 sodium salicylate 1 1 water 78.1 78.1 total 100 100

[0050] 1. Mix and stir polyhexamethylene biguanide, 2-bromo-2-nitro-1,3-propanediol and Tuoliron B with 50% of the above mass percent water for 3 hours to prepare a mixed substance A;

[0051] 2. Mix butyl iodopropynyl carbamate, sodium benzoate, sodium salicylate, and ethanol with the remaining 50% of the above mass percentage and stir for 3 hours to prepare mixed substance B;

[0052] 3. Stir and react the above mixed substance A with the above mixed substance B for 2 hours, then let it stand for 2 hours, and mix the mixed substance

[0053] The content of the mixture is determined, and the qualified mixture is packaged as a qualified produc...

Embodiment 3

[0055] components kilogram kg Mass percentage % polyhexamethylene biguanide 3 3 Polyhexamethyleneguanidine 7 7 Torrey B 0.3 0.3 2-Bromo-2-nitro-1,3-propanediol 1 1 95% ethanol 10 10 Butyl iodopropynylcarbamate 0.6 0.6 sodium gluconate 1.5 1.5 sodium salicylate 1.5 1.5 water 75.1 75.1 total 100 100

[0056] 1. Mix polyhexamethylene biguanide, polyhexamethylene guanidine, 2-bromo-2-nitro-1,3-propanediol and Tuoliron B with 50% of the above mass percent water Stirred for 3 hours to prepare mixed substance A;

[0057] 2. Mix butyl iodopropynylcarbamate, sodium gluconate, sodium salicylate, and ethanol with the remaining 50% of the above-mentioned mass percentage and stir for 3 hours to prepare a mixed substance B;

[0058] 3. Stir and react the above mixed substance A with the above mixed substance B for 2 hours, then let it stand for 2 hours, and mix the mixed substance

[0059] The content of...

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PUM

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Abstract

The invention aims to provide a compound leather bactericidal and mildew-proof agent, and in particular provides a preparation method taking the composition of a guanidine compound, 2-bromo-2-nitro-1,3-propanediol, 3-iodo-2-propynyl butylcarbamate, ethylenediaminetetraacetic acid (EDTA) B, a corrosion inhibitor, ethanol and water as the compound leather bactericidal and mildew-proof agent. The compound leather bactericidal and mildew-proof agent comprises the following components by mass percent: 1-15% of guanidine compound, 0.05-3% of EDTA B, 0.1-2% of 2-bromo-2-nitro-1,3-propanediol, 1-50% of ethanol, 0.05-5% of 3-iodo-2-propynyl butylcarbamate, 0.1-20% of corrosion inhibitor and the balance of water. The preparation method is characterized by comprising the following steps of: mixing the guanidine compound, the 2-bromo-2-nitro-1,3-propanediol and the EDTA B with 50% of water by mass percent, and stirring the mixture for 3 hours to prepare a mixture A; mixing the 3-iodo-2-propynyl butylcarbamate, the corrosion inhibitor and the ethanol with the residual 50% of water by mass percent, and stirring the mixture for 3 hours to prepare a mixture B; and stirring the mixture A and the mixture B to react for 2 hours, then standing for 2 hours, determining the content of the mixture of the mixture A and the mixture B, and packaging the qualified mixture, thus obtaining a qualified product. The invention also aims to dilute the compound leather bactericidal and mildew-proof agent, and the dilution ratio is 50-500 times.

Description

technical field [0001] The invention belongs to the field of disinfection and sterilization products, and relates to a compound sterilization and anti-mildew preparation of leather, especially a preparation of guanidine compounds, 2-bromo-2-nitro-1,3-propanediol, iodopropynyl carbamic acid The composition of butyl ester, Torlon B, corrosion inhibitor, ethanol and water is used as a compound fungicide and antifungal agent for leather. Background technique [0002] Leather raw materials are rich in nutrients such as protein and fat, which are easily invaded by microorganisms during storage, and are prone to mildew during processing. hotbed. [0003] The porosity and polar structure of the leather structure make it easy to absorb moisture and make the leather acidic. These factors constitute the basic conditions for mildew. Mildewed leather shows white, blue and black colonies and stains. The mold on the surface will develop into the interior of the leather over time, affecti...

Claims

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Application Information

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IPC IPC(8): A01N47/44A01N47/12A01N33/20A01P1/00A01P3/00
Inventor 李新建
Owner 覃终
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