PE (polyurethane) protective film glue and preparation method thereof
A technology of protective film and glue, applied in the direction of adhesive, film/sheet adhesive, adhesive type, etc., can solve the problems of water-based adhesive adhesion, bonding strength and drying time that are not as good as solvent-based adhesives, etc. The effect of fast drying time, strong adhesion and strong bond strength
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Embodiment 1
[0065] The formula used to prepare PE protective film glue is as follows:
[0066] Butyl acrylate (BA) 25
[0067] Methyl methacrylate (MMA) 45
[0068] Methyl acrylate (MA) 12
[0069] Acrylic (AA) 5
[0070] Hydroxyethyl acrylate (HEA) 20
[0071] Isooctyl acrylate (EHA) 120
[0072] Polyoxyethylene octyl phenyl ether (OP-10) 1.5
[0073] Sodium lauryl sulfate (SLS-046) 0.5
[0074] Sodium dodecylbenzene sulfonate 0.2
[0075] Deionized water 280
[0076] Ammonium persulfate 0.8
[0077] Polyisocyanates 2.3.
[0078] The preparation method is as follows:
[0079] S100. Preparation of seed emulsion: butyl acrylate, methyl methacrylate, methyl acrylate, and isooctyl acrylate that account for 30% of each weight in the formula, sodium lauryl sulfate and ten Add sodium dialkylbenzene sulfonate, initiator, and deionized water into the reactor, increase the temperature to 85°C, and keep it for 20 minutes;
[0080] S200. P...
Embodiment 2
[0087] The formula used to prepare PE protective film glue is as follows:
[0088] Butyl acrylate (BA) 40
[0089] Methyl methacrylate (MMA) 30
[0090] Methyl acrylate (MA) 20
[0091] Acrylic (AA) 10
[0092] Hydroxyethyl acrylate (HEA) 10
[0093] Isooctyl acrylate (EHA) 140
[0094] Octyl phenyl polyoxyethylene ether (OP-10) 0.9
[0095] Sodium Lauryl Sulfate (SLS-046) 1.0
[0096] Sodium dodecylbenzene sulfonate 0.7
[0097] Deionized water 350
[0098] Ammonium persulfate 1.5
[0099] Polyisocyanates 3.
[0100] The preparation method is as follows:
[0101] S100. Preparation of seed emulsion: butyl acrylate, methyl methacrylate, methyl acrylate, and isooctyl acrylate that account for 20% of each weight in the formula, sodium lauryl sulfate and ten Add sodium dialkylbenzene sulfonate, initiator, and deionized water into the reactor, increase the temperature to 80°C, and keep it for 30 minutes;
[0102] S200. Prepar...
Embodiment 3
[0109] The formula used to prepare PE protective film glue is as follows:
[0110] Butyl acrylate (BA) 55
[0111] Methyl methacrylate (MMA) 25
[0112] Methyl acrylate (MA) 30
[0113] Acrylic (AA) 15
[0114] Hydroxyethyl acrylate (HEA) 23
[0115] Isooctyl acrylate (EHA) 130
[0116] Polyoxyethylene octyl phenyl ether (OP-10) 0.5
[0117] Sodium Lauryl Sulfate (SLS-046) 1.5
[0118] Sodium dodecylbenzene sulfonate 1.5
[0119] Deionized water 300
[0120] Ammonium persulfate 0.6
[0121] Polyisocyanates 1.
[0122] The preparation method is as follows:
[0123] S100. Preparation of seed emulsion: butyl acrylate, methyl methacrylate, methyl acrylate, and isooctyl acrylate that account for 20% of each weight in the formula, and sodium lauryl sulfate and ten Add sodium dialkylbenzene sulfonate, initiator, and deionized water into the reactor, raise the temperature to 80°C, and keep it for 25 minutes;
[0124] S200. Prep...
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