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Preparation of indium-tin oxide/PDMS(polydimethylsiloxane) resin conducting material based on textile template

A technology of indium tin oxide and conductive materials, which is applied in the direction of oxide conductors, conductive layers on insulating carriers, circuits, etc., can solve the problems that there are no research reports on indium tin oxide/PDMS resin composite flexible conductive materials, and achieve Good electrical conductivity, simple production process, and good foldability

Inactive Publication Date: 2012-09-05
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, there is no research report on the preparation of indium tin oxide / PDMS resin composite flexible conductive materials based on textile templates

Method used

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  • Preparation of indium-tin oxide/PDMS(polydimethylsiloxane) resin conducting material based on textile template
  • Preparation of indium-tin oxide/PDMS(polydimethylsiloxane) resin conducting material based on textile template
  • Preparation of indium-tin oxide/PDMS(polydimethylsiloxane) resin conducting material based on textile template

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Weigh 0.5330g of indium chloride tetrahydrate and 0.0652g of tin chloride pentahydrate and dissolve them in 15ml of deionized water in a beaker, add NaOH (10wt%) to adjust the pH of the solution to 10.5, mix well, and transfer the reaction solution to the reaction In the kettle, react at 80° C. for 12 hours, cool naturally to room temperature, wash with deionized water and absolute ethanol for 3 times, and obtain an indium tin oxide precursor solution. Put the precursor solution into a Petri dish, and in a vacuum environment with a vacuum pump pressure of 0.08MPa, take 2.5g of cotton cloth and soak it repeatedly and dry it for 3 times, soak for 6 hours each time, dry at 65°C for 20 minutes, and then put it in a muffle Calcining in a furnace at 450° C. for 12 hours to obtain an indium tin oxide conductive material. Mix PDMS and supporting curing agent evenly at a mass ratio of 10:1, then spread the indium tin oxide conductive material on it, and cure it at 120°C for 10 m...

Embodiment 2

[0030] Take by weighing 2.4202g indium chloride tetrahydrate, 0.2980g tin chloride pentahydrate and dissolve in 50ml deionized water in a beaker, add ammonia water (28wt%) to adjust the pH of the solution=8.5, after mixing evenly, transfer the reaction solution to the reaction In the kettle, react at 60° C. for 15 h, cool down to room temperature naturally, wash repeatedly with deionized water 4 times, and wash repeatedly with absolute ethanol twice to obtain an indium tin oxide precursor solution. Put the precursor solution into a petri dish, and in a vacuum environment with a vacuum pump pressure of 0.1 MPa, take 1.8 g of non-woven fabrics and soak them repeatedly and dry them for 3 times, each soaking for 4 hours, drying at 80°C for 20 minutes, and then Calcining at 500° C. for 10 h in a muffle furnace to obtain an indium tin oxide conductive material. Mix PDMS and the supporting curing agent evenly at a mass ratio of 10:1, then spread the indium tin oxide conductive materi...

Embodiment 3

[0032]Take by weighing 1.9127g indium chloride tetrahydrate, 0.2632g tin chloride pentahydrate and dissolve in 40ml deionized water in a beaker, add NaOH (30wt%) to adjust the pH of the solution=11, after mixing evenly, transfer the reaction solution to the reaction In the kettle, react at 90°C for 8 hours, cool naturally to room temperature, wash repeatedly with deionized water 8 times, and wash repeatedly with absolute ethanol twice to obtain an indium tin oxide precursor solution. Put the precursor solution into a Petri dish, and in a vacuum environment with a vacuum pump pressure of 0.07MPa, take 2.1g of non-woven fabric and soak it repeatedly and dry it twice, soak for 6 hours each time, dry at 50°C for 40 minutes, and then Calcining at 550° C. for 10 h in a muffle furnace to obtain an indium tin oxide conductive material. Mix PDMS and supporting curing agent evenly at a mass ratio of 10:1, then spread the indium tin oxide conductive material on it, and cure it at 110°C f...

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Abstract

The invention relates to a method for preparing an indium-tin oxide / PDMS(polydimethylsiloxane) resin conducting material based on a textile template, which comprises the steps of: (1) preparing a precursor solution of an indium-tin oxide; (2) under a vacuumized environment, soaking a textile in the precursor solution, then taking out and drying, and calcining to obtain the indium-tin oxide conducting material; and (3) evenly mixing PDMS with a curing agent in a mass ratio of 10:1, then flatly laying the indium-tin oxide conducting material obtained in step (2) on the top of the mixture, curing at the temperature of 100 to 120 DEG C for 10 to 20min, and obtaining the indium-tin oxide / PDMS resin composite conducting material. The method provided by the invention has the advantages of simplepreparation process, low cost and easiness for realization of industrial production, and the prepared indium-tin oxide / PDMS resin composite flexible conducting material has the advantages of compact structure, fine electrical conductivity, fine foldable performance and broad market prospects.

Description

technical field [0001] The invention belongs to the field of preparation of conductive materials, in particular to a method for preparing indium tin oxide / PDMS resin conductive materials based on textile templates. Background technique [0002] In recent years, with the rapid development of information technology and optoelectronic products, new conductive materials have received more and more extensive research and attention. The research on transparent conductive oxide (TCO) is earlier, but it has attracted people's attention because of its excellent electrical conductivity, high chemical stability and good bonding performance with the substrate, especially in the field of electronics. Such as flat panel displays, sensors, dye-sensitized solar cells, etc. TCO materials mainly include SnO 2 Base, In 2 o 3 Various systems such as base and ZnO base, among which indium tin oxide (ITO) is the most representative. ITO is one of the most widely researched and applied transpa...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01B13/00H01B1/08H01B5/14
Inventor 王宏志胡沛然李耀刚张青红
Owner DONGHUA UNIV
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