Production method for sapphire pattern substrate
A graphic substrate and manufacturing method technology, applied in semiconductor/solid-state device manufacturing, electrical components, circuits, etc., can solve the problems of low yield of LED chips, difficult control of the manufacturing process, and limitation of the internal quantum efficiency of light-emitting diodes, etc., to achieve The effect of reducing the cost of making PSS, the preparation method is simple and diverse, and the preparation process is easy to control
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Embodiment 1
[0029] A kind of manufacture method of sapphire pattern substrate, concrete steps are:
[0030] (1), on the upper surface of the 2-inch C-face sapphire substrate, utilize chemical vapor deposition to grow a layer of low-refractive index material, a film with a thickness of 500 angstroms, and the material of the film is silicon nitride (SiN);
[0031] (2), prepare hemispherical mask on silicon nitride film with photoresist;
[0032] (3) By dry etching, the hemispherical photoresist mask pattern is transferred to the silicon nitride film, and hemispherical silicon nitride protrusions are formed on the sapphire substrate. The silicon nitride material between the hemispheres Etched clean to expose the sapphire substrate;
[0033] (4), with 150 degrees Celsius No. 3 solution (H 2 SO 4 :H 2 o 2 =3:1) to clean the sapphire substrate to prepare a sapphire pattern substrate.
[0034] The pattern of the gallium nitride-based light-emitting diode epitaxial substrate formed through ...
Embodiment 2
[0036] A kind of manufacture method of sapphire pattern substrate, concrete steps are:
[0037] (1), on the upper surface of the 2-inch sapphire substrate, utilize chemical vapor deposition to grow a layer of low-refractive index material, a film with a thickness of 400 angstroms, and the material of the film is silicon dioxide (SiO 2 );
[0038] (2), prepare conical mask on silicon dioxide thin film with photoresist;
[0039] (3) By dry etching, the conical photoresist mask pattern is transferred to the silicon dioxide film, and the conical silicon dioxide protrusions are formed on the sapphire substrate, and the silicon dioxide material between the cones Etched clean to expose the sapphire substrate;
[0040] (4), with 150 degrees Celsius No. 3 solution (H 2 SO 4 :H 2 o 2 =3:1) to clean the sapphire substrate to prepare a sapphire pattern substrate.
[0041] The pattern of the gallium nitride-based light-emitting diode epitaxial substrate formed through the above step...
Embodiment 3
[0043] A kind of manufacture method of sapphire pattern substrate, concrete steps are:
[0044] (1), on the upper surface of the 2-inch C-plane sapphire substrate, utilize chemical vapor deposition to grow a layer of low-refractive index material, a film with a thickness of 1 angstrom, and the material of the film is silicon nitride (SiN);
[0045] (2), prepare hemispherical mask on silicon nitride film with photoresist;
[0046] (3) By dry etching, the hemispherical photoresist mask pattern is transferred to the silicon nitride film, and hemispherical silicon nitride protrusions are formed on the sapphire substrate. The silicon nitride material between the hemispheres Etched clean to expose the sapphire substrate;
[0047] (4), with 150 degrees Celsius No. 3 solution (H 2 SO 4 :H 2 o 2 =3:1) to clean the sapphire substrate to prepare a sapphire pattern substrate.
[0048] The pattern of the gallium nitride-based light-emitting diode epitaxial substrate formed through th...
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