Fused silica ceramic material containing holmium oxide and preparation method thereof
A technology of fused silica and ceramic materials, applied in the field of high temperature structural ceramics
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Embodiment 1
[0017] The raw materials used in the fused silica ceramic material containing holmium oxide and the weight percentage of the raw materials are: 97.5% of fused silica fine powder <0.043mm, and 2.5% of holmium oxide fine powder <0.030mm. The fused silica fine powder and the holmium oxide fine powder are measured according to the proportion and then dry-mixed for 2 minutes, then gradually add 7% of polyvinyl alcohol solution with a mass concentration of 2% (percentage by weight, added) under constant stirring, and continue to stir and mix for 3 Pass through a 40-mesh sieve after 1 minute, continue to stir for 1 minute after sieving, and place the material in a sealed plastic bag to trap the material. After 4 hours of trapping the material, obtain a blank that can be used for pressure molding. The blank is formed by a hydraulic press, and the forming pressure of the blank is 100MPa. The molded green body was dried at room temperature of 20°C for 4 hours, then dried at 70°C for 1 h...
Embodiment 2
[0020] The raw materials used in the fused silica ceramic material containing holmium oxide and the weight percentage of the raw materials are: 98.5% of fused silica fine powder <0.043mm, and 1.5% of holmium oxide fine powder <0.030mm. The fused silica fine powder and the holmium oxide fine powder are measured according to the proportion and then dry-mixed for 2 minutes, then gradually add 7% of polyvinyl alcohol solution with a mass concentration of 2% (percentage by weight, added) under constant stirring, and continue to stir and mix for 3 Pass through a 40-mesh sieve after 1 minute, continue to stir for 1 minute after sieving, and place the material in a sealed plastic bag to trap the material. After 4 hours of trapping the material, obtain a blank that can be used for pressure molding. The blank is formed by a hydraulic press, and the forming pressure of the blank is 100MPa. The molded green body was dried at room temperature of 20°C for 4 hours, then dried at 70°C for 1 h...
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