Sintered neodymium-iron-boron magnethigh cost performance and high corrosion resistancepreparation method thereof
A technology of high corrosion resistance and sintered magnets, applied in the fields of magnetic objects, inductors/transformers/magnets, magnetic materials, etc., can solve problems such as difficult control, easy segregation of copper liquid phase sintering, and difficulty in preparing high-performance magnets for mass production. , to achieve the effect of high corrosion resistance and weight loss reduction
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Embodiment 1
[0020] Composition by design (PrNd) 29.55 Dy 2.2 Nb 0.3 Al 0.3 Ga 0.1 Cu 0.2 co 0.7 Ni 0.2 B 1.01 Fe 65.74 The raw materials are prepared and smelted in a 200kg flake furnace. The linear speed of the roller is 2-5m / s when the scales are poured, and finally the scales with a thickness of 0.25-0.35mm are obtained. Put these scales into a 500kg rotary hydrogen crushing furnace for hydrogen crushing, first absorb hydrogen under a hydrogen pressure of 70-90kPa for 1.5-3.5 hours, then vacuum dehydrogenate at about 530°C for 3-5 hours, reach about 5Pa, and cool for 8~ 12 hours. Add 0.1% antioxidant to the hydrogen crushed coarse powder, then in N 2 Enter the QLM300-5 jet mill under protection, the oxygen content of the jet mill is 100-150ppm, and obtain 3-3.5μm fine powder. Mix fine powder, gasoline and antioxidant uniformly in a mixer to get mixed powder. Among them, gasoline is No. 120 aviation gasoline, accounting for 2 to 3% of the total, and the molecular formula of ...
Embodiment 2
[0026] Composition by design (PrNd) 26.8 Dy 4.0 Nb 0.3 Al 0.2 Ga 0.1 Cu 0.15 co 1.2 B 1.01 Fe 66.24 Raw materials were prepared, and the unit price of the raw materials is listed in Table 2. The cost of the formula was 110.3 yuan / kg, and the sintered magnet was produced according to the process of Example 1. Measure the density and magnetic properties of the magnet produced by this method after machining, and do PCT (high pressure cooking test) detection. The PCT experimental conditions are the same as in Example 1, and the test results are listed in Table 3.
[0027] Table 2. Raw material unit price list
[0028] material name
Embodiment 3
[0034] Composition by design (PrNd) 23.7 Dy 8.4 Nb 0.5 al 0.7 Cu 0.02 co 0.6 B 1.05 Fe 63.86 Raw materials were prepared, and a sintered magnet was obtained according to the process of Example 1. Measure the density and magnetic properties of the magnet produced by this method after machining, and do PCT (high pressure cooking test) detection. The PCT experimental conditions are the same as in Example 1, and the test results are listed in Table 4.
[0035] Table 4. Experimental data comparison
[0036]
[0037] invention
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