Effervescent tablet of plant growth regulator composition and preparation method thereof

A plant growth regulator and growth regulator technology, applied in the directions of plant growth regulators, plant growth regulators, botanical equipment and methods, etc., can solve phytotoxicity, agricultural production losses, and accurate stability of active ingredients in water preparation products Quantitative difficulties and other problems, to achieve the effect of rapid disintegration, sufficient dissolution, and reducing the occurrence of phytotoxicity

Active Publication Date: 2010-03-03
CHINA AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the high moisture absorption and deliquescence of the mepiperium original drug, the composition loses its commercial value. On the other hand, the amount of active ingredients used in the early stage of crop growth is small, and it is difficult to accurately quantify and easily cause phytotoxicity during field operations, which brings great harm to agricultural production. loss; aqueous products also have certain difficulties in the stability of active ingredients and accurate quantification of field operations

Method used

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  • Effervescent tablet of plant growth regulator composition and preparation method thereof
  • Effervescent tablet of plant growth regulator composition and preparation method thereof
  • Effervescent tablet of plant growth regulator composition and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Example 1 Preparation of 0.2% diethyl diethyl ethyl methylpiperium effervescent tablet

[0037] The former drug diethyl hexanoate selects the 98.0% diethyl hexanoate former powder produced by Henan Zhengzhou Zhengshi Chemical Co., Ltd., and the former drug methylpiperium selects the 97.0% methylpiperium former powder produced by Jiangsu Changzhou Jiangnan Pesticide Factory (the following examples are the same) .

[0038] The selection and proportioning of the original drug and auxiliary agents are: 0.102 parts by mass of 98% diethyl hexanoate original drug (0.1 part by mass of pure), 0.104 parts by mass of 97.0% methylpiperium original drug (0.1 part by mass of pure), water blocking agent 0.1 parts by mass of diatomaceous earth, 30.0 parts by mass of acid effervescent agent oxalic acid, 30.0 parts by mass of alkaline effervescent agent sodium bicarbonate, 3.0 parts by mass of binder lactose, 5.0 parts by mass of glidant talc, 31.694 parts by mass of filler white carbon ...

Embodiment 2

[0050] Example 2 Preparation of 20% diethyl aminoethyl hexanoate mepiperium effervescent tablet

[0051] The selection and proportioning of the original drug and auxiliary agents are: 15.3 parts by mass of 98% diethyl hexanoate (15.0 parts by mass in pure form), 5.2 parts by mass of 97.0% methylpiperium original drug (5.0 parts by mass in pure form), water blocking agent 5.0 parts by mass of calcium carbonate, 10.0 parts by mass of acidic effervescent agent citric acid, 10.0 parts by mass of alkaline effervescent agent potassium bicarbonate, 3.0 parts by mass of binder carboxymethyl cellulose, 5.0 parts by mass of glidant calcium stearate , 46.5 parts by mass of filler kaolin.

[0052] Based on the preparation of a 10 kg sample, the dosage of each component is calculated and weighed according to the above proportions. Prepared by wet granulation and then tabletting, the method is as follows:

[0053] (1) After drying 1.53 kg of diethyl hexanoate and 0.52 kg of methylpiperium...

Embodiment 3、27

[0061] Embodiment 3, the preparation of 27.5% diethyl aminoethyl methylpiperium effervescent tablet

[0062] The selection and proportioning of the original drug and auxiliary agents are: 2.6 parts by mass of 98% diethyl ethyl hexanoate (2.5 parts by mass in pure form), 25.8 parts by mass of 97.0% methylpiperium technical product (25.0 parts by mass in pure form), water blocking agent 10.0 parts by mass of calcium hydrogen phosphate, 12.0 parts by mass of acid effervescent agent tartaric acid, 8.0 parts by mass of alkaline effervescent agent potassium carbonate, 3.0 parts by mass of binder polyethylene glycol, 3.0 parts by mass of glidant magnesium stearate, filler 35.6 parts by mass of bentonite.

[0063] Calculate and weigh the dosage of each component according to the above proportioning ratio. It is prepared by the direct dry compression method, and the specific process is the same as in Example 1.

[0064] The weight of each tablet of the prepared effervescent tablet is...

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Abstract

The invention discloses an effervescent tablet of a plant growth regulator composition and a preparation method thereof. The effervescent tablet of the plant growth regulator composition is made of the raw materials including the substances based on the parts by mass: 0.1-30 parts of diethyl aminoethyl hexanoate, 0.1-60 parts of mepiquat chloride, more than 0 part and less than or equal to 40 parts of water-blocking agent, 3-30 parts of acidic effervescence agent, 3-30 parts of alkaline effervescence agent, 1-10 parts of binding agent and 1-20 parts of glidant. The effervescent tablet can be prepared by a direct drying tabletting method or a wet granulation and secondary tabletting method, wherein the direct drying tabletting method can be used for preparing the effervescent tablet by mechanically grinding auxiliary agent, evenly mixing the auxiliary agent and two active components and directly tabletting; and the wet granulation and secondary tabletting method can be used for preparing the effervescent tablet by drying the two active components, grinding the auxiliary agent, preparing acidic and alkaline soft materials by mixing, bonding and pelleting, and finally tabletting. Thewater-blocking agent is introduced to solve the problem of moisture absorption of active ingredient solid preparation of mepiquat chloride; furthermore, the prepared mepiquat chloride composition effervescent tablet of the plant growth regulator diethyl aminoethyl hexanoate is a new formulation product having the characteristics of rapid disintegration, completely dissolving out of the active ingredient and accurate and quantitative field operation.

Description

technical field [0001] The invention relates to an effervescent tablet of a plant growth regulating composition and a preparation method thereof. Background technique [0002] At present, in agricultural production, lodging and yield increase are the main problems of cotton, soybean, peanut, rapeseed and other crops. [0003] Patent ZL 03118724.2 reports a plant growth regulator composition containing diethylaminoethanol hexanoate and methylpiperium as active ingredients. The composition can effectively prevent crops such as soybeans and cotton from lodging, and has a good effect of increasing yield and improving quality significantly , and the production process is simple and easy to use. [0004] Diethylaminoethanol hexanoate, commonly known as diethyl aminohexanoate, is a new type of plant metabolism regulator. Diethylaminoethanol can promote the growth of crop seedlings, enhance photosynthesis and material transfer, and promote the development of production organs such ...

Claims

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Application Information

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IPC IPC(8): A01N25/34A01N25/08A01N43/40A01N37/12A01P21/00
Inventor 段留生谭伟明朱晓峰李召虎周繁田晓莉翟志席何钟佩
Owner CHINA AGRI UNIV
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