Polycondensation production technology of melamine moulding particles and melamine moulding powder

A technology of molding particles and process technology, which is applied in the field of plastic production technology, and can solve problems such as high energy consumption, low density, and human body damage

Inactive Publication Date: 2010-02-24
任志广
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method is labor-intensive, consumes a lot of energy, pollutes the environment, and is harmful to the human body. The finished product has a lot of dust, low density, poor appearance, and it is difficult to effectively improve the quality and output.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0006] The specific implementation of the present invention will be further described below in conjunction with the examples.

[0007] The slurry preparation stage is carried out in the slurry reactor. Add 60 parts of formaldehyde, 3 parts of ammonium toluenesulfonate, 4 parts of methanol and 5 parts of water into the slurry reactor, heat up and stir. When the thermometer shows that the temperature of the material reaches 50°C, take a sample to test the pH value, determine the addition of urotropine according to the pH value, and adjust the pH value of the material to 8.0-8.5. During this process, the material continues to react and heat up. When the temperature reaches 60°C, add 40 parts of melamine into the slurry reactor, and then fully turn on the steam to heat up to boiling at the fastest speed. When the slurry boils, the temperature of the thermometer generally shows 95~ 97°C. After the slurry is boiled for 15 minutes, take a sample of 30ml for measurement, and decide ...

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PUM

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Abstract

The invention relates to a polycondensation production technology of melamine moulding particles and melamine moulding powder. The technology comprises the following steps: 1. in the slurry preparation phase, adding 55-65 parts of formaldehyde, 3-5 parts of thinner and 3-5 parts of water in a slurry reaction tank, heating and stirring, adjusting the pH value of slurry to 8.0-8.5 at 50 DEG C, adding 35-45 parts of melamine at 60 DEG C, heating for boiling to ensure the ratio of material to water to be 1:2, then performing cooling water circulation to reduce the temperature of material to 30-40DEG C, adding additives of which each accounts for 5-8 parts, stirring evenly, filtrating to prepare the desired slurry; 2. in the evaporation and polycondensation phase, adding the slurry in a vacuumwet pelletizing reaction tank, stirring at high speed, adding additives of which each accounts for 3-5% and 30-40% of auxiliary material, heating the materials to 70 DEG C to perform polymerization for 40min, breaking vacuum, reducing the temperature to 60 DEG C, discharging to obtain the finished melamine moulding particles; in addition, adding the melamine moulding particles in a grinder to grind to obtain the melamine moulding powder with the fineness of 80-100 meshes. The sealing production cycle is four hours, the charging powder yield is 60%, the water content of the finished product is3-5% and the cost of the finished product per ton is reduced by 500-900 RMB.

Description

technical field [0001] The invention relates to a plastic production process, in particular to a production process of molding particles and molding powder. Background technique [0002] Melamine molding granules and melamine molding powder are commonly used plastic basic raw materials, and are widely used in the manufacture of thermosetting plastics and rigid plastic structural parts. In recent years, due to the shortage of natural resources, the market demand for hard plastics has continued to expand, and the development prospects are good. At present, the production process of domestic melamine molding powder is to use formaldehyde and melamine as raw materials. It is pulped by integrating with wood pulp and dried in a mesh bag drying box to form a plate mold material, which is then crushed and ball milled to make a compact powder. Amine molding powder, the whole production process takes about 8 hours. This method is labor-intensive, consumes a lot of energy, pollutes t...

Claims

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Application Information

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IPC IPC(8): C08G12/32C08K3/22C08K3/30C08K5/098C08K5/42C08K5/101
Inventor 任志广
Owner 任志广
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