Method for preparing TiCl4 from titanium-containing furnace slag
A technology of titanium slag and slag, which is applied in the field of intermediate products prepared from titanium-containing slag, can solve the problems of complex growing process, increased slag viscosity, and affecting the quality of the furnace, and achieves short process flow, low reduction temperature, and resource utilization. high effect
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Embodiment 1
[0017] Using TiO 2 Titanium-containing slag with a content of 38.31% is used as a raw material, and the titanium-containing slag is about 3 kg. Anthracite is used as a reducing agent. Crush titanium-containing slag and anthracite to 80 mesh to 200 mesh and mix until uniform, mix 170ml of polyvinyl alcohol solution (prepared with water and polyvinyl alcohol 20:1) and 320ml of water as a binder, and mix the homogeneous The titanium-containing slag mixture and the binder are put into a disc pelletizer to prepare balls, and the particle size of the balls is 10-12mm. The prepared pellets were dried naturally and put into a silicon molybdenum rod resistance furnace, fed with nitrogen gas with a flow rate of 2L / min, and kept at 1350°C for 4 hours.
Embodiment 2
[0019] Using TiO 2 Titanium-containing slag with a content of 34.7% is used as raw material, about 50kg of titanium-containing slag, 11kg of coke powder is used as a reducing agent, the titanium-containing slag and coke powder are crushed to 80 mesh to 200 mesh and mixed until uniform, and water glass is used as a binder , the amount of water glass added is 5% of the titanium-containing slag, and the titanium-containing slag, coke powder, and water glass are mixed uniformly in the grinding pan, and the material ball is prepared on the ball press machine, and the pressed ball is an ellipsoid (about 5 cm long and wide About 3cm, about 2cm high). The prepared pellets were put into graphite crucible after natural drying, and the graphite crucible was put into a tunnel kiln for reduction and nitriding treatment. Nitrogen gas with a flow rate of 18L / min was introduced and kept at 1500°C for 8 hours.
Embodiment 3
[0021] Using TiO 2 Titanium-containing slag with a content of 45% is used as raw material, about 85kg of titanium-containing slag, 30kg of bituminous coal as a reducing agent, bentonite as a binder, and the addition amount is 1.5% of the titanium-containing slag, and the titanium-containing slag and bituminous coal are crushed to 100 Between ~200 mesh and mix with bentonite until uniform, add water in a disc pelletizer to form pellets, the particle size of the pellets is 6-8mm. The prepared pellets are put into the shaft furnace, and the pellets are dried on the top of the shaft furnace. Nitrogen gas with a flow rate of 21 L / min is introduced into the lower part of the shaft furnace, and reduction nitriding is carried out in the high temperature zone in the middle of the shaft furnace. The reduction nitriding temperature is 1200 ~1250°C, reduction time 6 hours.
[0022] Table 1 Chemical composition of anthracite %
[0023] Element FCd Vd ad S content 78...
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