Micro arc oxidation electrolytic solution for light metals and micro arc oxidation method
A technology of micro-arc oxidation and electrolyte, applied in anodic oxidation, etc., can solve the problems of poor scratch resistance and compactness, achieve good scratch resistance and compactness, high corrosion resistance and electrical insulation, and increase added value Effect
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Embodiment 1
[0027] This example illustrates the micro-arc oxidation electrolyte and the micro-arc oxidation method provided by the present invention.
[0028] Processing workpiece: aluminum alloy mobile phone battery cover
[0029] Material model: A16063
[0030] 1. Degreasing
[0031] The above-mentioned aluminum alloy workpiece is immersed in an alkaline solution containing 30 g / L sodium hydroxide, 40 g / L sodium phosphate, and 20 g / L sodium silicate to degrease the aluminum alloy base material. The degreasing temperature is 85° C., and the degreasing time is 8 minutes. Then wash with water for 5 minutes.
[0032] 2. Micro-arc oxidation: Immerse the above-mentioned degreased aluminum alloy workpiece into an electrolyte containing 25 g / L of sodium hexametaphosphate, 8 g / L of sodium silicate, 8 g / L of ammonium metavanadate, and 2 g / L of cobalt sulfate solution, and adjust the pH value to about 7.8 with 1.5 g / L sodium hydroxide. The aluminum alloy workpiece is used as the anode, the st...
Embodiment 2
[0037] This example illustrates the micro-arc oxidation electrolyte and the micro-arc oxidation method provided by the present invention.
[0038] Carry out micro-arc oxidation to the workpiece according to the method described in Example 1, the difference is that the electrolyte contains 25 grams per liter of sodium hexametaphosphate, 8 grams per liter of sodium silicate, 8 grams per liter of ammonium metavanadate, cobalt sulfate 2 g / L, glycerol 10 mL / L, sodium tungstate 1 g / L aqueous solution, the time of micro-arc oxidation is 10 minutes.
[0039] A product with a black micro-arc oxidation film was obtained, and the thickness of the formed film measured by a coating thickness gauge (PHYNIX, Pocket-Surfix, Germany) was 15 microns.
Embodiment 3
[0041] According to the method described in Example 1, the aluminum alloy workpiece is subjected to micro-arc oxidation. The difference is that the electrolyte contains 40 grams / liter of sodium hexametaphosphate, 10 grams / liter of sodium aluminate, 5 grams / liter of sodium silicate, and 5 grams / liter of metasilicate. An aqueous solution of 20 g / L ammonium vanadate, 0.1 g / L cobalt sulfate, 5 g / L sodium phosphate, 1 mL / L ethylenediamine, and 0.3 g / L sodium molybdate; the micro-arc oxidation time is 35 minutes.
[0042]Obtain the product that is attached to the aluminum alloy workpiece of black micro-arc oxidation film, measure the thickness of the formed film with coating thickness gauge (Germany PHYNIX company, Pocket-Surfix) and be 40 microns.
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