Synthesis technique of dual-component wet and heat ageing resistant epoxy building structure strengthening adhesive
A technology for building structure and heat and humidity resistance, applied in the field of structural reinforcement adhesive, can solve the problems of low initial bonding strength, poor heat and humidity aging resistance, unfavorable reinforcement, etc., and achieve excellent heat and humidity aging resistance, wide applicable temperature range, waterproof good gas performance
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Embodiment 1
[0029] (1), the preparation of component A:
[0030] a. Add active toughening agent polysulfide rubber JLY-1211 parts and liquid epoxy resin E51100 parts by weight to the stirrer, and stir for 3 to 5 minutes at room temperature at 700 rpm.
[0031] b. Then add reactive diluent E-108 parts, PGE 6 parts and defoamer Defom 68000.3 parts in order by weight, and stir at room temperature at 700 rpm for 3 to 5 minutes until they are evenly mixed.
[0032] c. Add 1 part of silane coupling agent KH5601 parts by weight to the liquid described in step (1) b, and stir evenly at room temperature;
[0033] d. Add 1 part of hydrophobic fumed white carbon black in parts by weight to the liquid described in step (1) c, stir evenly until no visible powder, then stir at 1400-2000 rpm for 15 minutes at high speed, and let it stand for defoaming. A component;
[0034] (2), preparation of component B
[0035] a. In the reaction vessel, 90 parts by weight of IPDA and 10 parts of MXDA were mixed u...
Embodiment 2
[0041] In the first component of embodiment one, the liquid epoxy resin E-51 is changed into 12880 parts, the hydrophobic fumed silica is changed into 2 parts, the reactive diluent E-10 is changed into 6 parts, and the reactive diluent PGE is changed into 8 parts, The active toughening agent polysulfide rubber JLY-121 is changed to 0.6 parts, the silane coupling agent KH560 is changed to 1.5 parts; the materials and parts by weight in component B are changed to: 75 parts of IPDA, 25 parts of MXDA, 70 parts of phenylethyl alcohol, salicylic acid 10 parts of acid, 5 parts of epoxy resin E-4425.
[0042] The weight ratio of curing agent and accelerator DMP-30 in component B is 45:2.
[0043] All the other and preparation method are with embodiment one
Embodiment 3
[0045] In the component A of Example 1: liquid epoxy resin 128 is changed to 120 parts, defoamer Defom 6800 is changed to 0.8 parts, reactive diluent is changed to E10 7 parts, PGE 7 parts, active toughening agent polysulfide rubber JLY -121 is changed to 1.5 parts, the silane coupling agent KH560 is changed to 2 parts; the materials and parts by weight in component B are changed to: 95 parts of IPDA, 5 parts of MXDA, 85 parts of benzyl alcohol, 12 parts of salicylic acid, epoxy resin E-4425 copies. The ratio of accelerator DMP-30 and curing agent in component B is 3:80.
[0046] The rest and the preparation method are the same as in Example 1.
[0047] Performance test data of embodiment one, two, three and domestic and foreign similar products
[0048] actual project
actual conditions
foreign products
domestic product
Embodiment one
Embodiment two
Embodiment three
Tensile Strength
(MPA)
7 days at room temperature
...
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