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Microwave rotating thin film concentrator

A technology of rotating thin film and concentrator, which is applied in forced circulation evaporators, chemical instruments and methods, lighting and heating equipment, etc., can solve the problems of low heat transfer efficiency, bumping, decomposition, etc., achieve wide application prospects, increase evaporation Area, the effect of expanding the scope of application

Inactive Publication Date: 2008-08-06
PHARM TECH TIANJIN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Traditional single-effect concentrators and multi-effect concentrators have long heating time and low heat transfer efficiency, and the active ingredients are exposed to high-temperature environments for a long time, causing decomposition; traditional heat exchangers use Plate or tube method, the surface is difficult to clean and easy to structure, resulting in low heat transfer efficiency and serious heat loss; at the same time, when the material is evaporated, the bubbles will cause serious bumping, and the material liquid is often lost. In order to achieve effective concentration, it must be Appropriately reducing the vacuum degree will further cause the concentration speed to be slow and the loss of components will increase

Method used

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  • Microwave rotating thin film concentrator
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Effect test

Embodiment 1

[0014] Microwave rotary thin film concentrator, including airtight tank 1, rotary evaporator 2, microwave generator 3, solution feed pipe 4, concentrate liquid discharge pipe 5, condenser 6, microwave shielding device 7, stirring motor 8 and vacuum system.

[0015] The main body of the microwave rotary thin film concentrator is a closed tank body, which is a cylindrical cavity with an openable cover, a sight glass on the cover, and a microwave shielding device on the inner surface of the observation window; a microwave device is placed in the closed tank At the inner wall; the tank body has an opening, and the opening is connected to the condenser, and the condenser is connected to the vacuum system through a pipeline. A rotating thin-film concentrator is placed in the center of the tank. The evaporation surface of the evaporator is designed in a conical shape. The evaporator cone angle b is 180°; the angle a between the axis of the evaporator and the horizontal plane is 90°. ...

Embodiment 2

[0017] Microwave rotary thin film concentrator, including airtight tank 1, rotary evaporator 2, microwave generator 3, solution feed pipe 4, concentrate liquid discharge pipe 5, condenser 6, microwave shielding device 7, stirring motor 8 and vacuum system.

[0018] The main body of the microwave rotary thin film concentrator is a closed tank body, which is a cylindrical cavity with an openable cover, a sight glass on the cover, and a microwave shielding device on the inner surface of the observation window; the microwave device is placed on the inner wall of the closed tank There are 2 places; the tank body has an opening, and the opening is connected to the condenser, and the condenser is connected to the vacuum system through a pipeline. A rotating thin-film concentrator is placed in the center of the tank. The evaporation surface of the evaporator is designed in a conical shape. The evaporator cone angle b is 60°; the angle a between the axis of the evaporator and the horiz...

Embodiment 3

[0020] Microwave rotary thin film concentrator, including airtight tank 1, rotary evaporator 2, microwave generator 3, solution feed pipe 4, concentrate liquid discharge pipe 5, condenser 6, microwave shielding device 7, stirring motor 8 and vacuum system.

[0021] The main body of the microwave rotary thin-film concentrator is a closed tank body, which is a cylindrical cavity with an openable cover. There are 2 sight glasses on the cover, and there is a microwave shielding device on the inner surface of the observation window; a microwave device is placed in the The solution feed pipe outside the closed tank body; the tank body has an opening, which is connected to the condenser, and the condenser is connected to the vacuum system through a pipeline. A rotating thin-film concentrator is placed in the center of the tank. The evaporation surface of the evaporator is designed in a conical shape. The evaporator cone angle b is 120°; the angle a between the axis of the evaporator ...

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Abstract

The invention discloses a microwave rotating film concentration device, comprising a sealing tank body (1), a rotating evaporator (2), a microwave device (3), a solution feeding tube (4), a concentrated liquid discharging tube (5), condenser (6), a microwave shielding device (7), a stirring motor (8) and a vacuum system; wherein the evaporating surface of the rotating evaporator (2) is conical or round, the angle a between the axis of the evaporator and the horizontal plane is 0 to 90 degree, the rotating evaporator (2) adopts a magnetic stirring device to be connected with the external stirring motor (8), which is arranged in the center of the sealing tank body which is provided with a cover which can be opened and closed, the cover is provided with a sight glass (9). The concentration device solves the problems of the present equipments in the process of concentrating extraction liquid, such as the low evaporating speed, the high concentrating temperature, the decomposition of feed solution caused by long-term heating, decompression operation being impossible because of the blasting boiling of feed solution, the low energy utilization ratio, the large size of equipment, and the equipment being difficult to be cleaned, thus the invention has a wide applied prospect.

Description

technical field [0001] The invention relates to a concentration device, in particular to a microwave rotary film concentration device. Background technique [0002] Concentration technology is widely used in the evaporation of liquids and the crystallization of compounds, mainly in atmospheric pressure concentration, reduced pressure concentration and freeze-drying methods. The main way of decompression is to reduce the evaporation temperature of the material under reduced pressure, and after the thermal energy is supplied to the liquid, the solvent is evaporated, so as to effectively increase the concentration and promote the crystallization. [0003] Traditional single-effect concentrators and multi-effect concentrators have long heating time and low heat transfer efficiency, and the active ingredients are exposed to high-temperature environments for a long time, causing decomposition; traditional heat exchangers use plate or tube methods, and the surface is difficult to c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D1/00
CPCB01D1/0017B01D1/0094B01D1/223F26B5/041F26B5/048F26B17/284
Inventor 孙小兵张文生吴海花
Owner PHARM TECH TIANJIN
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